[3,4-bis(difluoromethoxy)phenyl]-{4-[2-((2-trimethylsilylethoxy)methoxy)propane-2-yl]phenyl} chloromethane

Base Information

Chemical Name:[3,4-bis(difluoromethoxy)phenyl]-{4-[2-((2-trimethylsilylethoxy)methoxy)propane-2-yl]phenyl} chloromethane
CAS No.:1055709-57-3
Molecular Formula:C₂₄H₃₁ClF₄O₄Si
Molecular Weight:523.04
Hs Code.:

Synonyms:[3,4-bis(difluoromethoxy)phenyl]-{4-[2-((2-trimethylsilylethoxy)methoxy)propane-2-yl]phenyl} chloromethane

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Chemical Property of [3,4-bis(difluoromethoxy)phenyl]-{4-[2-((2-trimethylsilylethoxy)methoxy)propane-2-yl]phenyl} chloromethane

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Technology Process of [3,4-bis(difluoromethoxy)phenyl]-{4-[2-((2-trimethylsilylethoxy)methoxy)propane-2-yl]phenyl} chloromethane

There total 5 articles about [3,4-bis(difluoromethoxy)phenyl]-{4-[2-((2-trimethylsilylethoxy)methoxy)propane-2-yl]phenyl} chloromethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1055709-54-0
[3,4-bis(difluoromethoxy)phenyl]-{4-[2-((2-trimethylsilylethoxy)methoxy)propane-2yl]phenyl}methanol

: 1055709-57-3
[3,4-bis(difluoromethoxy)phenyl]-{4-[2-((2-trimethylsilylethoxy)methoxy)propane-2-yl]phenyl} chloromethane

Guidance literature:: With pyridine; thionyl chloride; In toluene; at 0 ℃;
DOI:10.1016/S0960-894X(02)00190-7

Reference yield:

: 106-37-6
1.4-dibromobenzene

: 1055709-57-3
[3,4-bis(difluoromethoxy)phenyl]-{4-[2-((2-trimethylsilylethoxy)methoxy)propane-2-yl]phenyl} chloromethane

Guidance literature:: Multi-step reaction with 4 steps

1: n-BuLi / tetrahydrofuran / -78 °C

2: iPr₂NEt / CH₂Cl₂

3: n-BuLi / tetrahydrofuran

4: SOCl₂; pyridine / toluene / 0 °C

With pyridine; n-butyllithium; thionyl chloride; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane; toluene;
DOI:10.1016/S0960-894X(02)00190-7

Reference yield:

: 127842-54-0
3,4-bis-(difluoromethoxy)-benzaldehyde

: 1055709-57-3
[3,4-bis(difluoromethoxy)phenyl]-{4-[2-((2-trimethylsilylethoxy)methoxy)propane-2-yl]phenyl} chloromethane

Guidance literature:: Multi-step reaction with 2 steps

1: n-BuLi / tetrahydrofuran

2: SOCl₂; pyridine / toluene / 0 °C

With pyridine; n-butyllithium; thionyl chloride; In tetrahydrofuran; toluene;
DOI:10.1016/S0960-894X(02)00190-7