C₂₃H₃₅NO₃

Base Information

• Chemical Name: C₂₃H₃₅NO₃
• CAS No.: 628724-30-1
• Molecular Formula: C₂₃H₃₅NO₃
• Molecular Weight: 373.536
• Mol file: 628724-30-1.mol

Synonyms:C₂₃H₃₅NO₃

Chemical Property of C₂₃H₃₅NO₃

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₃H₃₅NO₃

There total 12 articles about C₂₃H₃₅NO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

cycloxexanone dimethyl ketal (933-40-4) → C23H35NO3 (628724-30-1)

Guidance literature:

Multi-step reaction with 3 steps

1: 85 percent / p-toluenesulfonic acid monohydrate / dimethylformamide / 2 h / 20 °C

2: 90 percent / m-chloroperbenzoic acid; sodium dihydrogen phosphate; sodium hydrogen phosphate / CH₂Cl₂; H₂O / 3 h / 0 °C / pH 6

3: 66 percent / propan-2-ol / 144 h / 120 °C

With disodium hydrogenphosphate; sodium dihydrogen phosphate; toluene-4-sulfonic acid; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; water; N,N-dimethyl-formamide; isopropyl alcohol;

DOI:10.1016/j.bmc.2004.09.023

Reference yield:

3,4-di-O-acetyl-2,6-dibromo-2,6-dideoxy-5a-carba-β-L-glucopyranosyl bromide → C23H35NO3 (628724-30-1)

Guidance literature:

Multi-step reaction with 8 steps

1.1: 32 percent / zinc; acetic acid / 2 h / 80 °C

2.1: sodium methoxide / methanol / 1 h / 20 °C

3.1: pyridine / 15 h / 0 °C

3.2: 0.87 g / 4-dimethylaminopyridine / 17 h / 20 °C

4.1: dimethylformamide; H₂O / 15 h / 110 °C

5.1: 0.34 g / sodium methoxide / methanol / 3 h / 20 °C

6.1: 85 percent / p-toluenesulfonic acid monohydrate / dimethylformamide / 2 h / 20 °C

7.1: 90 percent / m-chloroperbenzoic acid; sodium dihydrogen phosphate; sodium hydrogen phosphate / CH₂Cl₂; H₂O / 3 h / 0 °C / pH 6

8.1: 66 percent / propan-2-ol / 144 h / 120 °C

With pyridine; disodium hydrogenphosphate; sodium dihydrogen phosphate; sodium methylate; toluene-4-sulfonic acid; acetic acid; 3-chloro-benzenecarboperoxoic acid; zinc; In methanol; dichloromethane; water; N,N-dimethyl-formamide; isopropyl alcohol; 2.1: Zemplen de-O-acetylation / 5.1: Zemplen de-O-acylation;

DOI:10.1016/j.bmc.2004.09.023

Reference yield:

1,5-anhydro-3,4-O-(cyclohexane-1,1-diyl)-2,6-dideoxy-5a-carba-L-lyxo-hex-1-enitol (828268-88-8) → C23H35NO3 (628724-30-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 90 percent / m-chloroperbenzoic acid; sodium dihydrogen phosphate; sodium hydrogen phosphate / CH₂Cl₂; H₂O / 3 h / 0 °C / pH 6

2: 66 percent / propan-2-ol / 144 h / 120 °C

With disodium hydrogenphosphate; sodium dihydrogen phosphate; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; water; isopropyl alcohol;

DOI:10.1016/j.bmc.2004.09.023

upstream raw materials:

4-phenyl-1-butylamine

C₁₃H₂₀O₃

1,5-anhydro-3,4-O-(cyclohexane-1,1-diyl)-2,6-dideoxy-5a-carba-L-lyxo-hex-1-enitol

cycloxexanone dimethyl ketal