acetic acid 5-acetoxy-6-acetoxymethyl-4-[7-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-8-(4-methoxy-benzyloxy)-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-6-yloxy]-2-(2-trimethylsilanyl-ethoxy)-tetrahydro-pyran-3-yl ester

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Chemical Name:acetic acid 5-acetoxy-6-acetoxymethyl-4-[7-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-8-(4-methoxy-benzyloxy)-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-6-yloxy]-2-(2-trimethylsilanyl-ethoxy)-tetrahydro-pyran-3-yl ester
CAS No.:373648-17-0
Molecular Formula:C₄₆H₅₅NO₁₆Si
Molecular Weight:906.025
Hs Code.:

acetic acid 5-acetoxy-6-acetoxymethyl-4-[7-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-8-(4-methoxy-benzyloxy)-2-phenyl-hexahydro-pyrano[3,2-<i>d</i>][1,3]dioxin-6-yloxy]-2-(2-trimethylsilanyl-ethoxy)-tetrahydro-pyran-3-yl ester

Synonyms:acetic acid 5-acetoxy-6-acetoxymethyl-4-[7-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-8-(4-methoxy-benzyloxy)-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-6-yloxy]-2-(2-trimethylsilanyl-ethoxy)-tetrahydro-pyran-3-yl ester

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Chemical Property of acetic acid 5-acetoxy-6-acetoxymethyl-4-[7-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-8-(4-methoxy-benzyloxy)-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-6-yloxy]-2-(2-trimethylsilanyl-ethoxy)-tetrahydro-pyran-3-yl ester

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Technology Process of acetic acid 5-acetoxy-6-acetoxymethyl-4-[7-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-8-(4-methoxy-benzyloxy)-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-6-yloxy]-2-(2-trimethylsilanyl-ethoxy)-tetrahydro-pyran-3-yl ester

There total 1 articles about acetic acid 5-acetoxy-6-acetoxymethyl-4-[7-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-8-(4-methoxy-benzyloxy)-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-6-yloxy]-2-(2-trimethylsilanyl-ethoxy)-tetrahydro-pyran-3-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 143746-87-6
Phenyl 4,6-O-benzylidene-2-deoxy-3-O-(4-methoxybenzyl)-2-phthalimido-1-thio-β-D-glucopyranoside

: Acetic acid (2R,3R,4S,5R,6R)-5-acetoxy-6-acetoxymethyl-4-hydroxy-2-(2-trimethylsilanyl-ethoxy)-tetrahydro-pyran-3-yl ester

: 373648-17-0
acetic acid 5-acetoxy-6-acetoxymethyl-4-[7-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-8-(4-methoxy-benzyloxy)-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-6-yloxy]-2-(2-trimethylsilanyl-ethoxy)-tetrahydro-pyran-3-yl ester

Guidance literature:: With N-iodo-succinimide; trifluorormethanesulfonic acid; 4 A molecular sieve; In dichloromethane; at -20 ℃;
DOI:10.1081/CAR-100104868

Reference yield: 91.0%

: 108-24-7
acetic anhydride

: 93-97-0
benzoic acid anhydride

: 373648-17-0
acetic acid 5-acetoxy-6-acetoxymethyl-4-[7-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-8-(4-methoxy-benzyloxy)-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-6-yloxy]-2-(2-trimethylsilanyl-ethoxy)-tetrahydro-pyran-3-yl ester

: 373648-18-1
C₅₅H₆₁NO₁₅Si

Guidance literature:: acetic acid 5-acetoxy-6-acetoxymethyl-4-[7-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-8-(4-methoxy-benzyloxy)-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-6-yloxy]-2-(2-trimethylsilanyl-ethoxy)-tetrahydro-pyran-3-yl ester; With hydrazine hydrate; In ethanol; for 24h; Heating;

acetic anhydride; In methanol;

benzoic acid anhydride; With dmap;
DOI:10.1081/CAR-100104868

Reference yield:

: 373648-17-0
acetic acid 5-acetoxy-6-acetoxymethyl-4-[7-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-8-(4-methoxy-benzyloxy)-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-6-yloxy]-2-(2-trimethylsilanyl-ethoxy)-tetrahydro-pyran-3-yl ester

: C₄₈H₅₇NO₁₅Si

Guidance literature:: Multi-step reaction with 2 steps

1.1: NH₂NH₂*H₂O / ethanol / 24 h / Heating

1.2: methanol

1.3: 91 percent / DMAP

2.1: AcOH / H₂O

With hydrazine hydrate; acetic acid; In ethanol; water;
DOI:10.1081/CAR-100104868