methyl(2,4,6-trimethylphenyl)thiocarbamic acid (S)-1-phenyl-ethyl ester

Base Information

Chemical Name:methyl(2,4,6-trimethylphenyl)thiocarbamic acid (S)-1-phenyl-ethyl ester
CAS No.:1292296-58-2
Molecular Formula:C₁₉H₂₃NOS
Molecular Weight:313.464
Hs Code.:

Synonyms:methyl(2,4,6-trimethylphenyl)thiocarbamic acid (S)-1-phenyl-ethyl ester

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Chemical Property of methyl(2,4,6-trimethylphenyl)thiocarbamic acid (S)-1-phenyl-ethyl ester

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Technology Process of methyl(2,4,6-trimethylphenyl)thiocarbamic acid (S)-1-phenyl-ethyl ester

There total 3 articles about methyl(2,4,6-trimethylphenyl)thiocarbamic acid (S)-1-phenyl-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 1292296-35-5
1-methyl-3-[methyl(2,4,6-trimethylphenyl)carbamoyl]-3H-imidazol-1-ium iodide

: 62258-06-4,67385-07-3,133098-85-8
thioacetic acid S-((S)-1-phenylethyl) ester

: 1292296-58-2
methyl(2,4,6-trimethylphenyl)thiocarbamic acid (S)-1-phenyl-ethyl ester

Guidance literature:: thioacetic acid S-((S)-1-phenylethyl) ester; With lithium aluminium tetrahydride; In tetrahydrofuran; diethyl ether; Reflux;

With hydrogenchloride; water; In tetrahydrofuran; diethyl ether;

1-methyl-3-[methyl(2,4,6-trimethylphenyl)carbamoyl]-3H-imidazol-1-ium iodide; With triethylamine; In dichloromethane; for 20h;
DOI:10.1039/c0cc04912c

Reference yield:

: 1292296-29-7
imidazole-1-carboxylic acid methyl(2,4,6-trimethylphenyl)amide

: 1292296-58-2
methyl(2,4,6-trimethylphenyl)thiocarbamic acid (S)-1-phenyl-ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: acetonitrile / 4 h / Reflux

2.1: lithium aluminium tetrahydride / tetrahydrofuran; diethyl ether / Reflux

2.3: 20 h

With lithium aluminium tetrahydride; In tetrahydrofuran; diethyl ether; acetonitrile;
DOI:10.1039/c0cc04912c

Reference yield:

: 13021-14-2
N-methyl-2,4,6-trimethylaniline

: 1292296-58-2
methyl(2,4,6-trimethylphenyl)thiocarbamic acid (S)-1-phenyl-ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: tetrahydrofuran / 96 h / Reflux

2.1: acetonitrile / 4 h / Reflux

3.1: lithium aluminium tetrahydride / tetrahydrofuran; diethyl ether / Reflux

3.3: 20 h

With lithium aluminium tetrahydride; In tetrahydrofuran; diethyl ether; acetonitrile;
DOI:10.1039/c0cc04912c