(+)-(1S,2S,5S)-6-allyl-2-methoxy-8-(2,4-dimethoxybenzyl)-6,8-diazabicyclo[3.2.2]nonane-7,9-dione

Base Information

Chemical Name:(+)-(1S,2S,5S)-6-allyl-2-methoxy-8-(2,4-dimethoxybenzyl)-6,8-diazabicyclo[3.2.2]nonane-7,9-dione
CAS No.:1134635-39-4
Molecular Formula:C₂₀H₂₆N₂O₅
Molecular Weight:374.437
Hs Code.:

Synonyms:(+)-(1S,2S,5S)-6-allyl-2-methoxy-8-(2,4-dimethoxybenzyl)-6,8-diazabicyclo[3.2.2]nonane-7,9-dione

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Chemical Property of (+)-(1S,2S,5S)-6-allyl-2-methoxy-8-(2,4-dimethoxybenzyl)-6,8-diazabicyclo[3.2.2]nonane-7,9-dione

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Technology Process of (+)-(1S,2S,5S)-6-allyl-2-methoxy-8-(2,4-dimethoxybenzyl)-6,8-diazabicyclo[3.2.2]nonane-7,9-dione

There total 1 articles about (+)-(1S,2S,5S)-6-allyl-2-methoxy-8-(2,4-dimethoxybenzyl)-6,8-diazabicyclo[3.2.2]nonane-7,9-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 1134584-26-1
(+)-(1S,2S,5S)-6-allyl-2-hydroxy-8-(2,4-dimethoxybenzyl)-6,8-diazabicyclo[3.2.2]nonane-7,9-dione

: 74-88-4
methyl iodide

: 1134635-39-4
(+)-(1S,2S,5S)-6-allyl-2-methoxy-8-(2,4-dimethoxybenzyl)-6,8-diazabicyclo[3.2.2]nonane-7,9-dione

Guidance literature:: (+)-(1S,2S,5S)-6-allyl-2-hydroxy-8-(2,4-dimethoxybenzyl)-6,8-diazabicyclo[3.2.2]nonane-7,9-dione; With sodium hydride; In tetrahydrofuran; paraffin oil; for 0.333333h; Inert atmosphere; Cooling with ice;

methyl iodide; In tetrahydrofuran; paraffin oil; at 20 ℃; for 16h; Inert atmosphere;
DOI:10.1016/j.bmc.2008.11.043

Reference yield: 25.0%

: 1134635-39-4
(+)-(1S,2S,5S)-6-allyl-2-methoxy-8-(2,4-dimethoxybenzyl)-6,8-diazabicyclo[3.2.2]nonane-7,9-dione

: 1134635-45-2
(-)-(1R,2S,5S)-6-allyl-2-methoxy-8-(2,4-dimethoxybenzyl)-6,8-diazabicyclo[3.2.2]nonane

Guidance literature:: (+)-(1S,2S,5S)-6-allyl-2-methoxy-8-(2,4-dimethoxybenzyl)-6,8-diazabicyclo[3.2.2]nonane-7,9-dione; With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 ℃; for 16.1667h; Reflux; Inert atmosphere;

With water; In tetrahydrofuran; at 0 ℃; for 0.666667h; Reflux;
DOI:10.1016/j.bmc.2008.11.043