2-bromo-1-fluoro-5-(3-(methylsulfonyl)propoxy)-3-(trifluoromethyl)benzene

Base Information

Chemical Name:2-bromo-1-fluoro-5-(3-(methylsulfonyl)propoxy)-3-(trifluoromethyl)benzene
CAS No.:1544739-73-2
Molecular Formula:C₁₁H₁₁BrF₄O₃S
Molecular Weight:379.17
Hs Code.:

Synonyms:2-bromo-1-fluoro-5-(3-(methylsulfonyl)propoxy)-3-(trifluoromethyl)benzene

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Chemical Property of 2-bromo-1-fluoro-5-(3-(methylsulfonyl)propoxy)-3-(trifluoromethyl)benzene

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Technology Process of 2-bromo-1-fluoro-5-(3-(methylsulfonyl)propoxy)-3-(trifluoromethyl)benzene

There total 1 articles about 2-bromo-1-fluoro-5-(3-(methylsulfonyl)propoxy)-3-(trifluoromethyl)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1544739-72-1
1-fluoro-3-(3-(methylsulfonyl)propoxy)-5-(trifluoromethyl)benzene

: 1544739-73-2
2-bromo-1-fluoro-5-(3-(methylsulfonyl)propoxy)-3-(trifluoromethyl)benzene

Guidance literature:: With bromine; acetic acid; at 20 ℃; for 4h;

Reference yield:

: 1544739-73-2
2-bromo-1-fluoro-5-(3-(methylsulfonyl)propoxy)-3-(trifluoromethyl)benzene

: 1544739-24-3
4-[2-fluoro-5-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-benzyloxy]-1,1a,6,6a-tetrahydro-3-aza-cyclopropa[a]indene-1-carboxylic acid ethyl ester

: 1544739-74-3
(5aR,6S,6aS)-ethyl 3-((2’,4-difluoro-4’-(3-(methylsulfonyl)propoxy)-6’-(trifluoromethyl)-[1,1‘-biphenyl]-3-yl)methoxy)-5,5a,6,6a-tetrahydrocyclopropa[4,5]-cyclopenta[1,2-c]pyridine-6-carboxylate

Guidance literature:: With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium phosphate; In tetrahydrofuran; water; at 100 ℃; for 0.166667h; Inert atmosphere; Sealed tube; Microwave irradiation;

Reference yield:

: 1544739-73-2
2-bromo-1-fluoro-5-(3-(methylsulfonyl)propoxy)-3-(trifluoromethyl)benzene

: 1544739-24-3
4-[2-fluoro-5-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-benzyloxy]-1,1a,6,6a-tetrahydro-3-aza-cyclopropa[a]indene-1-carboxylic acid ethyl ester

: 1544739-71-0
(5aR,6S,6aS)-3-((2’,4-difluoro-4’-(3-(methylsulfonyl)propoxy)-6’-(trifluoromethyl)-[1,1‘-biphenyl]-3-yl)methoxy)-5,5a,6,6a-tetrahydrocyclopropa[4,5]cyclopenta[1,2-c]pyridine-6-carboxylic acid

Guidance literature:: Multi-step reaction with 2 steps

1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium phosphate / tetrahydrofuran; water / 0.17 h / 100 °C / Inert atmosphere; Sealed tube; Microwave irradiation

2: lithium hydroxide monohydrate; water / tetrahydrofuran; methanol / 4 h / 20 °C

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium phosphate; lithium hydroxide monohydrate; water; In tetrahydrofuran; methanol; water;