1,4-dihydro-4-(3,4-dimethoxyphenyl)-2,6-dimethyl-1-(3-phenylpropyl)-3,5-pyridinecarboxylic acid 3-methyl-5-benzylester

Base Information

Chemical Name:1,4-dihydro-4-(3,4-dimethoxyphenyl)-2,6-dimethyl-1-(3-phenylpropyl)-3,5-pyridinecarboxylic acid 3-methyl-5-benzylester
CAS No.:170750-36-4
Molecular Formula:C₃₄H₃₇NO₆
Molecular Weight:555.671
Hs Code.:

Synonyms:1,4-dihydro-4-(3,4-dimethoxyphenyl)-2,6-dimethyl-1-(3-phenylpropyl)-3,5-pyridinecarboxylic acid 3-methyl-5-benzylester

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Chemical Property of 1,4-dihydro-4-(3,4-dimethoxyphenyl)-2,6-dimethyl-1-(3-phenylpropyl)-3,5-pyridinecarboxylic acid 3-methyl-5-benzylester

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Technology Process of 1,4-dihydro-4-(3,4-dimethoxyphenyl)-2,6-dimethyl-1-(3-phenylpropyl)-3,5-pyridinecarboxylic acid 3-methyl-5-benzylester

There total 3 articles about 1,4-dihydro-4-(3,4-dimethoxyphenyl)-2,6-dimethyl-1-(3-phenylpropyl)-3,5-pyridinecarboxylic acid 3-methyl-5-benzylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.2%

: 637-59-2
1-Bromo-3-phenylpropane

: 170750-35-3
1,4-dihydro-4-(3,4-dimethoxyphenyl)-2,6-dimethyl-3,5-pyridinedicarboxylic acid 3-methyl-5-benzylester

: 170750-36-4
1,4-dihydro-4-(3,4-dimethoxyphenyl)-2,6-dimethyl-1-(3-phenylpropyl)-3,5-pyridinecarboxylic acid 3-methyl-5-benzylester

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; at 100 ℃; for 1h;
DOI:10.1248/cpb.43.818

Reference yield:

: 120-14-9
3,4-dimethoxy-benzaldehyde

: 170750-36-4
1,4-dihydro-4-(3,4-dimethoxyphenyl)-2,6-dimethyl-1-(3-phenylpropyl)-3,5-pyridinecarboxylic acid 3-methyl-5-benzylester

Guidance literature:: Multi-step reaction with 3 steps

1: piperidine, acetic acid / benzene / 2 h / Heating

2: triethylamine / benzene / 3 h / Heating

3: 65.2 percent / NaH / dimethylformamide / 1 h / 100 °C

With piperidine; sodium hydride; acetic acid; triethylamine; In N,N-dimethyl-formamide; benzene;
DOI:10.1248/cpb.43.818

Reference yield:

: 1026584-12-2
2-[1-(3,4-Dimethoxy-phenyl)-meth-(Z)-ylidene]-3-oxo-butyric acid benzyl ester

: 170750-36-4
1,4-dihydro-4-(3,4-dimethoxyphenyl)-2,6-dimethyl-1-(3-phenylpropyl)-3,5-pyridinecarboxylic acid 3-methyl-5-benzylester

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / benzene / 3 h / Heating

2: 65.2 percent / NaH / dimethylformamide / 1 h / 100 °C

With sodium hydride; triethylamine; In N,N-dimethyl-formamide; benzene;
DOI:10.1248/cpb.43.818