C₂₃H₂₄INO₄

Base Information

Chemical Name:C₂₃H₂₄INO₄
CAS No.:1155288-13-3
Molecular Formula:C₂₃H₂₄INO₄
Molecular Weight:505.352
Hs Code.:

C<sub>23</sub>H<sub>24</sub>INO<sub>4</sub>

Synonyms:C₂₃H₂₄INO₄

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Chemical Property of C₂₃H₂₄INO₄

Chemical Property:

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Technology Process of C₂₃H₂₄INO₄

There total 13 articles about C₂₃H₂₄INO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 1155288-12-2
C₁₇H₁₉BrINO₃

: 108-95-2,27073-41-2
phenol

: 1155288-13-3
C₂₃H₂₄INO₄

Guidance literature:: phenol; With potassium carbonate; In N,N-dimethyl-formamide; for 1h;

C₁₇H₁₉BrINO₃; In N,N-dimethyl-formamide;

Reference yield:

: 1000995-00-5
C₁₄H₁₄ClNO₂

: 1155288-13-3
C₂₃H₂₄INO₄

Guidance literature:: Multi-step reaction with 9 steps

1.1: hydrogenchloride / tetrahydrofuran; 1,4-dioxane / 0.67 h / 20 °C

1.2: 16 h / Heating / reflux

1.3: 20 °C

2.1: potassium hexamethylsilazane / tetrahydrofuran; toluene / 0.5 h / -78 °C

2.2: 0.5 h / -78 °C

2.3: -78 - 20 °C

3.1: perchloric acid / 2 h / 20 °C

3.2: pH ~ 6

4.1: sodium hydroxide; water / ethanol / 4 h / 20 °C

4.2: pH ~ 3 - ~ 4

5.1: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 5.5 h / 30 - 35 °C

5.2: 16 h / 20 °C

6.1: lithium hydroxide; water; dihydrogen peroxide / tetrahydrofuran / 0.5 h / 0 °C

6.2: pH ~ 4 - ~ 5

7.1: diethyl ether

8.1: N-Bromosuccinimide / dibenzoyl peroxide / tetrachloromethane / 24 h / 75 °C

9.1: potassium carbonate / N,N-dimethyl-formamide / 1 h

With hydrogenchloride; lithium hydroxide; sodium hydroxide; N-Bromosuccinimide; perchloric acid; water; dihydrogen peroxide; potassium hexamethylsilazane; potassium carbonate; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; dibenzoyl peroxide; In tetrahydrofuran; 1,4-dioxane; tetrachloromethane; diethyl ether; ethanol; N,N-dimethyl-formamide; toluene;

Reference yield:

: 1155270-29-3
methyl (S)-2-(tert-butoxy)-2-(4-iodo-2-methylquinolin-3-yl)acetate

: 1155288-13-3
C₂₃H₂₄INO₄

Guidance literature:: Multi-step reaction with 2 steps

1: N-Bromosuccinimide / dibenzoyl peroxide / tetrachloromethane / 24 h / 75 °C

2: potassium carbonate / N,N-dimethyl-formamide / 1 h

With N-Bromosuccinimide; potassium carbonate; dibenzoyl peroxide; In tetrachloromethane; N,N-dimethyl-formamide;