[1-Chloro-1-(diisopropoxy-phosphoryl)-2-phenyl-ethyl]-phosphonic acid diisopropyl ester

Base Information

Chemical Name:[1-Chloro-1-(diisopropoxy-phosphoryl)-2-phenyl-ethyl]-phosphonic acid diisopropyl ester
CAS No.:101194-34-7
Molecular Formula:C₂₀H₃₅ClO₆P₂
Molecular Weight:468.895
Hs Code.:

Synonyms:[1-Chloro-1-(diisopropoxy-phosphoryl)-2-phenyl-ethyl]-phosphonic acid diisopropyl ester

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Chemical Property of [1-Chloro-1-(diisopropoxy-phosphoryl)-2-phenyl-ethyl]-phosphonic acid diisopropyl ester

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Technology Process of [1-Chloro-1-(diisopropoxy-phosphoryl)-2-phenyl-ethyl]-phosphonic acid diisopropyl ester

There total 3 articles about [1-Chloro-1-(diisopropoxy-phosphoryl)-2-phenyl-ethyl]-phosphonic acid diisopropyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 20107-67-9
tetraisopropyl esters of monochloromethylene bisphosphonic acid

: 100-39-0
benzyl bromide

: 101194-34-7
[1-Chloro-1-(diisopropoxy-phosphoryl)-2-phenyl-ethyl]-phosphonic acid diisopropyl ester

Guidance literature:: With thallium (I) ethoxide; sodium iodide; In tetrahydrofuran; for 2h; Heating;
DOI:10.1016/0022-328X(85)80161-3

Reference yield:

: 1660-95-3
Tetraisopropyl methylenediphosphonate

: 101194-34-7
[1-Chloro-1-(diisopropoxy-phosphoryl)-2-phenyl-ethyl]-phosphonic acid diisopropyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 82 percent / sodium hypochlorite

2: 71 percent / n-butyllithium

3: 82 percent / NaI, thallium(I) ethoxide / tetrahydrofuran / 2 h / Heating

With sodium hypochlorite; n-butyllithium; thallium (I) ethoxide; sodium iodide; In tetrahydrofuran;
DOI:10.1016/0022-328X(85)80161-3

Reference yield:

: 10596-22-2
tetraisopropyl dichloromethylenebisphosphonate

: 101194-34-7
[1-Chloro-1-(diisopropoxy-phosphoryl)-2-phenyl-ethyl]-phosphonic acid diisopropyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 71 percent / n-butyllithium

2: 82 percent / NaI, thallium(I) ethoxide / tetrahydrofuran / 2 h / Heating

With n-butyllithium; thallium (I) ethoxide; sodium iodide; In tetrahydrofuran;
DOI:10.1016/0022-328X(85)80161-3