2-(2,2-Diethoxyethoxy)toluene

Base Information

• Chemical Name: 2-(2,2-Diethoxyethoxy)toluene
• CAS No.: 117516-63-9
• Molecular Formula: C₁₃H₂₀O₃
• Molecular Weight: 224.3
• Mol file: 117516-63-9.mol

Synonyms:1-(2,2-diethoxyethoxy)-2-methylbenzene

Chemical Property of 2-(2,2-Diethoxyethoxy)toluene

Chemical Property:

• Boiling Point: 306.7±37.0 °C(Predicted)
• Density: 0.995±0.06 g/cm3(Predicted)

Purity/Quality:

99% ^*data from raw suppliers

2-(2,2-Diethoxyethoxy)toluene 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-(2,2-Diethoxyethoxy)toluene

There total 3 articles about 2-(2,2-Diethoxyethoxy)toluene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

ortho-cresol (95-48-7,77504-84-8) + Bromoacetaldehyde diethyl acetal (2032-35-1) → 1-(2,2-diethoxyethoxy)-2-methylbenzene (117516-63-9)

Guidance literature:

With potassium carbonate; In various solvent(s); at 150 ℃; for 5h;

DOI:10.1021/jm00003a014

Reference yield:

ortho-cresol (95-48-7,77504-84-8) + chloroacetaldehyde diethyl acetal (621-62-5) → 1-(2,2-diethoxyethoxy)-2-methylbenzene (117516-63-9)

Guidance literature:

With sodium ethanolate; at 180 ℃; im geschlossenen Rohr;

Reference yield:

sodium o-cresolate (4549-72-8) + chloroacetaldehyde diethyl acetal (621-62-5) → 1-(2,2-diethoxyethoxy)-2-methylbenzene (117516-63-9)

Guidance literature:

With diethylene glycol; at 150 ℃;

upstream raw materials:

ortho-cresol

chloroacetaldehyde diethyl acetal

sodium o-cresolate

Bromoacetaldehyde diethyl acetal

Downstream raw materials:

7-methylbenzofuran

2-(o-tolyloxymethyl)thiazolidine

7-methyl-2-benzofurancarboxaldehyde

4-[5-(7-methyl-benzofuran-2-yl)-1H-pyrrol-2-yl]-benzoic acid methyl ester