3-[4,4-bis(benzenesulfonyl)-1-hydroxybutyl]-5-butyl-2,5-dihydrofuran-2-one

Base Information

Chemical Name:3-[4,4-bis(benzenesulfonyl)-1-hydroxybutyl]-5-butyl-2,5-dihydrofuran-2-one
CAS No.:1432519-04-4
Molecular Formula:C₂₄H₂₈O₇S₂
Molecular Weight:492.614
Hs Code.:

Synonyms:3-[4,4-bis(benzenesulfonyl)-1-hydroxybutyl]-5-butyl-2,5-dihydrofuran-2-one

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Chemical Property of 3-[4,4-bis(benzenesulfonyl)-1-hydroxybutyl]-5-butyl-2,5-dihydrofuran-2-one

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Technology Process of 3-[4,4-bis(benzenesulfonyl)-1-hydroxybutyl]-5-butyl-2,5-dihydrofuran-2-one

There total 3 articles about 3-[4,4-bis(benzenesulfonyl)-1-hydroxybutyl]-5-butyl-2,5-dihydrofuran-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1432519-03-3
5-butyl-3-[1-hydroxy-4,4-bis(phenylsulfanyl)butyl]-3-(phenylselanyl)oxolan-2-one

: 1432519-04-4
3-[4,4-bis(benzenesulfonyl)-1-hydroxybutyl]-5-butyl-2,5-dihydrofuran-2-one

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 0 ℃; for 12h; Cooling with ice;
DOI:10.1039/c3ob40115d

Reference yield:

: 104-50-7
gamma-octalactone

: 1432519-04-4
3-[4,4-bis(benzenesulfonyl)-1-hydroxybutyl]-5-butyl-2,5-dihydrofuran-2-one

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium hexamethylsilazane / toluene; tetrahydrofuran / 0.75 h / -78 °C

1.2: 0.33 h / -78 °C

2.1: lithium diisopropyl amide / hexane; tetrahydrofuran / 0.75 h / -78 °C

2.2: 0.08 h

2.3: -78 °C

3.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 12 h / 0 °C / Cooling with ice

With potassium hexamethylsilazane; 3-chloro-benzenecarboperoxoic acid; lithium diisopropyl amide; In tetrahydrofuran; hexane; dichloromethane; toluene;
DOI:10.1039/c3ob40115d

Reference yield:

: 1432518-81-4
5-butyl-3-(phenylselanyl)oxolan-2-one

: 1432519-04-4
3-[4,4-bis(benzenesulfonyl)-1-hydroxybutyl]-5-butyl-2,5-dihydrofuran-2-one

Guidance literature:: Multi-step reaction with 2 steps

1.1: lithium diisopropyl amide / hexane; tetrahydrofuran / 0.75 h / -78 °C

1.2: 0.08 h

1.3: -78 °C

2.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 12 h / 0 °C / Cooling with ice

With 3-chloro-benzenecarboperoxoic acid; lithium diisopropyl amide; In tetrahydrofuran; hexane; dichloromethane;
DOI:10.1039/c3ob40115d