5-butyl-3-[1-hydroxy-4,4-bis(phenylsulfanyl)butyl]-3-(phenylselanyl)oxolan-2-one

Base Information

Chemical Name:5-butyl-3-[1-hydroxy-4,4-bis(phenylsulfanyl)butyl]-3-(phenylselanyl)oxolan-2-one
CAS No.:1432519-03-3
Molecular Formula:C₃₀H₃₄O₃S₂Se
Molecular Weight:585.69
Hs Code.:

Synonyms:5-butyl-3-[1-hydroxy-4,4-bis(phenylsulfanyl)butyl]-3-(phenylselanyl)oxolan-2-one

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Chemical Property of 5-butyl-3-[1-hydroxy-4,4-bis(phenylsulfanyl)butyl]-3-(phenylselanyl)oxolan-2-one

Chemical Property:

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Technology Process of 5-butyl-3-[1-hydroxy-4,4-bis(phenylsulfanyl)butyl]-3-(phenylselanyl)oxolan-2-one

There total 5 articles about 5-butyl-3-[1-hydroxy-4,4-bis(phenylsulfanyl)butyl]-3-(phenylselanyl)oxolan-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1432518-85-8
4,4-bis[(4-fluorophenyl)sulfanyl]butanal

: 1432518-81-4
5-butyl-3-(phenylselanyl)oxolan-2-one

: 1432519-03-3
5-butyl-3-[1-hydroxy-4,4-bis(phenylsulfanyl)butyl]-3-(phenylselanyl)oxolan-2-one

Guidance literature:: 5-butyl-3-(phenylselanyl)oxolan-2-one; With lithium diisopropyl amide; In tetrahydrofuran; hexane; at -78 ℃; for 0.75h;

With N,N,N,N,N,N-hexamethylphosphoric triamide; In tetrahydrofuran; hexane; for 0.0833333h;

4,4-bis[(4-fluorophenyl)sulfanyl]butanal; In tetrahydrofuran; hexane; at -78 ℃;
DOI:10.1039/c3ob40115d

Reference yield:

: 371-42-6
4-Fluorothiophenol

: 1432519-03-3
5-butyl-3-[1-hydroxy-4,4-bis(phenylsulfanyl)butyl]-3-(phenylselanyl)oxolan-2-one

Guidance literature:: Multi-step reaction with 4 steps

1.1: trifluoroacetic acid / dichloromethane / 24 h / 20 °C

2.1: tetra-(n-butyl)ammonium iodide / dimethyl sulfoxide / 24 h / 50 °C

3.1: diisobutylaluminium hydride / dichloromethane; toluene / 1.83 h / -78 - 0 °C / Cooling with ice

4.1: lithium diisopropyl amide / hexane; tetrahydrofuran / 0.75 h / -78 °C

4.2: 0.08 h

4.3: -78 °C

With tetra-(n-butyl)ammonium iodide; diisobutylaluminium hydride; trifluoroacetic acid; lithium diisopropyl amide; In tetrahydrofuran; hexane; dichloromethane; dimethyl sulfoxide; toluene;
DOI:10.1039/c3ob40115d

Reference yield:

: 1432519-38-4
1-({3-chloro-1-[(4-fluorophenyl)sulfanyl]propyl}sulfanyl)-4-fluorobenzene

: 1432519-03-3
5-butyl-3-[1-hydroxy-4,4-bis(phenylsulfanyl)butyl]-3-(phenylselanyl)oxolan-2-one

Guidance literature:: Multi-step reaction with 3 steps

1.1: tetra-(n-butyl)ammonium iodide / dimethyl sulfoxide / 24 h / 50 °C

2.1: diisobutylaluminium hydride / dichloromethane; toluene / 1.83 h / -78 - 0 °C / Cooling with ice

3.1: lithium diisopropyl amide / hexane; tetrahydrofuran / 0.75 h / -78 °C

3.2: 0.08 h

3.3: -78 °C

With tetra-(n-butyl)ammonium iodide; diisobutylaluminium hydride; lithium diisopropyl amide; In tetrahydrofuran; hexane; dichloromethane; dimethyl sulfoxide; toluene;
DOI:10.1039/c3ob40115d