3-O-benzyl-2-deoxy-4,5-O-isopropylidene-D-erythro-pentose dipropyl mercaptal

Base Information

Chemical Name:3-O-benzyl-2-deoxy-4,5-O-isopropylidene-D-erythro-pentose dipropyl mercaptal
CAS No.:111717-54-5
Molecular Formula:C₂₁H₃₄O₃S₂
Molecular Weight:398.631
Hs Code.:

Synonyms:3-O-benzyl-2-deoxy-4,5-O-isopropylidene-D-erythro-pentose dipropyl mercaptal

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-O-benzyl-2-deoxy-4,5-O-isopropylidene-D-erythro-pentose dipropyl mercaptal

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Technology Process of 3-O-benzyl-2-deoxy-4,5-O-isopropylidene-D-erythro-pentose dipropyl mercaptal

There total 1 articles about 3-O-benzyl-2-deoxy-4,5-O-isopropylidene-D-erythro-pentose dipropyl mercaptal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100-39-0
benzyl bromide

: 111689-69-1
2-deoxy-4,5-O-isopropylidene-D-erythro-pentose dipropyl mercaptal

: 111717-54-5
3-O-benzyl-2-deoxy-4,5-O-isopropylidene-D-erythro-pentose dipropyl mercaptal

Guidance literature:: With sodium hydride; Yield given. Multistep reaction; 1.) DMF, 0 - 5 deg C, 1 h, 2.) a) 0 - 5 deg C, 30 min b) RT, 3 h;
DOI:10.1021/jo00239a028

Reference yield: 97.0%

: 111717-54-5
3-O-benzyl-2-deoxy-4,5-O-isopropylidene-D-erythro-pentose dipropyl mercaptal

: 103795-36-4
(3S,4R)-3-O-benzyl-4,5-O-isopropylidene-3,4,5-trihydroxypentanal

Guidance literature:: With mercury dichloride; mercury(II) oxide; In water; acetonitrile; at 0 ℃; for 0.5h;
DOI:10.1021/jo00239a028

Reference yield:

: 111717-54-5
3-O-benzyl-2-deoxy-4,5-O-isopropylidene-D-erythro-pentose dipropyl mercaptal

: 111689-72-6
5-O-benzyl-2,3,4-trideoxy-6,7-O-isopopylidene-D-erythro-heptanoic acid ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 97 percent / HgCl₂, yellow HgO / acetonitrile; H₂O / 0.5 h / 0 °C

2: 1.) sodium hydride / 1.) THF, 25 deg C, 1 h, 2.) RT, 1 h

3: 91 percent / cyclohexene / 20percent Pd(OH)2/C / ethanol / 18 h / Heating

With sodium hydride; mercury dichloride; mercury(II) oxide; cyclohexene; palladium dihydroxide; In ethanol; water; acetonitrile;
DOI:10.1021/jo00239a028