dispirotrioxan-6',1''-cyclohexane>

Base Information

• Chemical Name: dispirotrioxan-6',1''-cyclohexane>
• CAS No.: 79258-08-5
• Molecular Formula: C₁₃H₂₂O₃
• Molecular Weight: 226.316

Synonyms:dispirotrioxan-6',1''-cyclohexane>

Chemical Property of dispirotrioxan-6',1''-cyclohexane>

Chemical Property:

Purity/Quality:

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MSDS Files:

SDS file from LookChem

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Technology Process of dispirotrioxan-6',1''-cyclohexane>

There total 2 articles about dispirotrioxan-6',1''-cyclohexane> which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 5.0%

1-oxaspiro(2.5)octane (185-70-6) + 1,1'-dihydroxycyclohexyl peroxide (2407-94-5) → Cyclohexanone diperoxide (183-84-6) + cyclohexanone (108-94-1,11119-77-0,9003-41-2,9075-99-4) + dispirotrioxan-6',1''-cyclohexane> (79258-08-5)

Guidance literature:

With chlorosulfonic acid; tungsten(VI) oxide; In dichloromethane; at 25 ℃; for 5h;

Reference yield:

1-oxaspiro(2.5)octane (185-70-6) + 1,1'-dihydroxycyclohexyl peroxide (2407-94-5) → cyclohexanone (108-94-1,11119-77-0,9003-41-2,9075-99-4) + dispirotrioxan-6',1''-cyclohexane> (79258-08-5)

Guidance literature:

With chlorosulfonic acid; tungsten(VI) oxide; Yield given. Multistep reaction. Yields of byproduct given; 1) CH₂Cl₂, 20 deg C, 3 h, 2) CH₂Cl₂, 2 h;

DOI:10.1039/c39810000581

Reference yield: 52.0%

dispirotrioxan-6',1''-cyclohexane> (79258-08-5) → (1-hydroxycyclohexyl)methyl 6-bromohexanoate + cyclohexanone (108-94-1,11119-77-0,9003-41-2,9075-99-4)

Guidance literature:

With iron(II) bromide; In tetrahydrofuran; at 20 ℃; for 16h;

DOI:10.1021/jo050385+

upstream raw materials:

1-oxaspiro(2.5)octane

1,1'-dihydroxycyclohexyl peroxide

Downstream raw materials:

cyclohexanone

2-Adamantanone

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