C₅H₅FeCO{P(OC₆H₅)3}{C(CH₃)C(CO₂CH₃)CH₃}

Base Information

Chemical Name:C₅H₅FeCO{P(OC₆H₅)3}{C(CH₃)C(CO₂CH₃)CH₃}
CAS No.:87556-52-3
Molecular Formula:C₃₀H₂₉FeO₆P
Molecular Weight:572.377
Hs Code.:

C<sub>5</sub>H<sub>5</sub>FeCO{P(OC<sub>6</sub>H<sub>5</sub>)3}{C(CH<sub>3</sub>)C(CO<sub>2</sub>CH<sub>3</sub>)CH<sub>3</sub>}

Synonyms:C₅H₅FeCO{P(OC₆H₅)3}{C(CH₃)C(CO₂CH₃)CH₃}

Suppliers and Price of C₅H₅FeCO{P(OC₆H₅)3}{C(CH₃)C(CO₂CH₃)CH₃}

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₅H₅FeCO{P(OC₆H₅)3}{C(CH₃)C(CO₂CH₃)CH₃}

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Technology Process of C₅H₅FeCO{P(OC₆H₅)3}{C(CH₃)C(CO₂CH₃)CH₃}

There total 1 articles about C₅H₅FeCO{P(OC₆H₅)3}{C(CH₃)C(CO₂CH₃)CH₃} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: {(Cp)iron(carbonyl){P(O(phenyl))3}}I

: 917-54-4
methyllithium

: 23326-27-4
Methyl 2-butynoate

: 87556-44-3
C₅H₅FeCO{P(OC₆H₅)3}{C(CO₂CH₃)C(CH₃)2}

: 87556-52-3
C₅H₅FeCO{P(OC₆H₅)3}{C(CH₃)C(CO₂CH₃)CH₃}

Guidance literature:: With copper(l) iodide; silver tetrafluoroborate; In tetrahydrofuran; (N2); mixt. of Fe complex and AgBF4 stirred in CH2Cl2 for 10 min, CH3C2CO2CH3 added, stirred for 15 min, filtered (Celite), evapd., dissolved in THF at -78°C, LiCu(CH3)2 (prepd. from CH3Li and CuI in THF at 0°C) added at -78°C,; allowed to warm to room temp., evapd., redissolved (CH2Cl2/pentane), chromd. (Al2O3, CH2Cl2/pentane), evapd.; elem. anal.;