1,2',6'-tri-N-benzyloxycarbonyl-2-O-(methylsulfonyl)fortimicin B 4,5-carbamate

Base Information

Chemical Name:1,2',6'-tri-N-benzyloxycarbonyl-2-O-(methylsulfonyl)fortimicin B 4,5-carbamate
CAS No.:76801-46-2
Molecular Formula:C₄₁H₅₀N₄O₁₄S
Molecular Weight:854.932
Hs Code.:

Synonyms:1,2',6'-tri-N-benzyloxycarbonyl-2-O-(methylsulfonyl)fortimicin B 4,5-carbamate

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Chemical Property of 1,2',6'-tri-N-benzyloxycarbonyl-2-O-(methylsulfonyl)fortimicin B 4,5-carbamate

Chemical Property:

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Technology Process of 1,2',6'-tri-N-benzyloxycarbonyl-2-O-(methylsulfonyl)fortimicin B 4,5-carbamate

There total 3 articles about 1,2',6'-tri-N-benzyloxycarbonyl-2-O-(methylsulfonyl)fortimicin B 4,5-carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 73236-63-2,76822-40-7
1,2',6'-tri-N-(benzyloxycarbonyl)fortimicin B 4,5-carbamate

: 7143-01-3
Methanesulfonic anhydride

: 76801-46-2
1,2',6'-tri-N-benzyloxycarbonyl-2-O-(methylsulfonyl)fortimicin B 4,5-carbamate

Guidance literature:: In pyridine; 1.) 1 h; 2.) overnight, RT;
DOI:10.1016/S0008-6215(00)80392-4

Reference yield:

: 66962-55-8,71658-13-4,76822-42-9,78609-41-3,78781-05-2
1,2',6'-tri-N-benzyloxycarbonylfortimicin B

: 76801-46-2
1,2',6'-tri-N-benzyloxycarbonyl-2-O-(methylsulfonyl)fortimicin B 4,5-carbamate

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / NaHCO₃ / methanol; H₂O / 3 h / Ambient temperature

2: 89 percent / NaHCO₃ / methanol / 1.5 h / Heating

3: 100 percent / pyridine / 1.) 1 h; 2.) overnight, RT

With sodium hydrogencarbonate; In pyridine; methanol; water;
DOI:10.1016/S0008-6215(00)80392-4

Reference yield:

: 78561-47-4
1,2',6'-tri-N-benzyloxycarbonyl-4-N-ethoxycarbonylfortimicin B

: 76801-46-2
1,2',6'-tri-N-benzyloxycarbonyl-2-O-(methylsulfonyl)fortimicin B 4,5-carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: 89 percent / NaHCO₃ / methanol / 1.5 h / Heating

2: 100 percent / pyridine / 1.) 1 h; 2.) overnight, RT

With sodium hydrogencarbonate; In pyridine; methanol;
DOI:10.1016/S0008-6215(00)80392-4