Technology Process of C25H24O5
There total 4 articles about C25H24O5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: (S)-2-{bis[3,5-bis(trifluoromethyl)phenyl][(trimethylsilanyl)oxy]methyl}pyrrolidine; dihydrogen peroxide / dichloromethane; water / 20 °C
2: benzene / 20 °C
3: diisobutylaluminium hydride / tetrahydrofuran / -78 °C
4: n-butyllithium; methanesulfonyl chloride; lithium bromide / tetrahydrofuran / -78 °C
5: sodium hydride / tetrahydrofuran / 0 - 20 °C
With
(S)-2-{bis[3,5-bis(trifluoromethyl)phenyl][(trimethylsilanyl)oxy]methyl}pyrrolidine; n-butyllithium; dihydrogen peroxide; sodium hydride; diisobutylaluminium hydride; methanesulfonyl chloride; lithium bromide;
In
tetrahydrofuran; dichloromethane; water; benzene;
2: Wittig reaction;
DOI:10.1021/ja2014604
- Guidance literature:
-
Multi-step reaction with 4 steps
1: benzene / 20 °C
2: diisobutylaluminium hydride / tetrahydrofuran / -78 °C
3: n-butyllithium; methanesulfonyl chloride; lithium bromide / tetrahydrofuran / -78 °C
4: sodium hydride / tetrahydrofuran / 0 - 20 °C
With
n-butyllithium; sodium hydride; diisobutylaluminium hydride; methanesulfonyl chloride; lithium bromide;
In
tetrahydrofuran; benzene;
1: Wittig reaction;
DOI:10.1021/ja2014604
- Guidance literature:
-
Multi-step reaction with 2 steps
1: n-butyllithium; methanesulfonyl chloride; lithium bromide / tetrahydrofuran / -78 °C
2: sodium hydride / tetrahydrofuran / 0 - 20 °C
With
n-butyllithium; sodium hydride; methanesulfonyl chloride; lithium bromide;
In
tetrahydrofuran;
DOI:10.1021/ja2014604
