C₂₇H₃₄O₂Si

Base Information

Chemical Name:C₂₇H₃₄O₂Si
CAS No.:1417803-56-5
Molecular Formula:C₂₇H₃₄O₂Si
Molecular Weight:418.651
Hs Code.:

C<sub>27</sub>H<sub>34</sub>O<sub>2</sub>Si

Synonyms:C₂₇H₃₄O₂Si

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Chemical Property of C₂₇H₃₄O₂Si

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Technology Process of C₂₇H₃₄O₂Si

There total 3 articles about C₂₇H₃₄O₂Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 1417803-51-0
(5S)-5-[(2S)-3-(tert-butyldiphenylsiloxy)-2-methylpropyl]furan-2(5H)-one

: 2622-05-1
allylmagnesium bromide

: 1417803-56-5
C₂₇H₃₄O₂Si

Guidance literature:: With copper(l) iodide; In tetrahydrofuran; at -78 ℃;
DOI:10.1016/j.tet.2012.11.077

Reference yield:

: 175272-36-3
(4R)-4-Benzyl-3-[(2S)-2-methyl-4-pentenoyl]-1,3-oxazolidin-2-one

: 1417803-56-5
C₂₇H₃₄O₂Si

Guidance literature:: Multi-step reaction with 6 steps

1.1: lithium aluminium tetrahydride / diethyl ether / 1 h / 0 °C / Inert atmosphere

2.1: 1H-imidazole / dichloromethane / 6 h / 0 - 20 °C

3.1: phosphonite ligand; tris(dibenzylideneacetone)diplatinum⁽⁰⁾; bis(pinacol)diborane / tetrahydrofuran / 12 h / 60 °C

3.2: 4 h / 0 - 20 °C

4.1: sodium hydrogencarbonate; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; potassium bromide; sodium hypochlorite / dichloromethane; water / 0.5 h / 0 °C / Inert atmosphere

5.1: sodium hydride / tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere

5.2: 3 h / -78 - 20 °C / Inert atmosphere

6.1: copper(l) iodide / tetrahydrofuran / -78 °C

With 1H-imidazole; sodium hypochlorite; copper(l) iodide; lithium aluminium tetrahydride; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; tris(dibenzylideneacetone)diplatinum⁽⁰⁾; phosphonite ligand; sodium hydride; sodium hydrogencarbonate; bis(pinacol)diborane; potassium bromide; In tetrahydrofuran; diethyl ether; dichloromethane; water; 5.1: |Wittig Olefination / 5.2: |Wittig Olefination;
DOI:10.1016/j.tet.2012.11.077

Reference yield:

: 5673-98-3,63501-27-9,88080-30-2,63501-26-8
(S)-(-)-2-methyl-4-penten-1-ol

: 1417803-56-5
C₂₇H₃₄O₂Si

Guidance literature:: Multi-step reaction with 5 steps

1.1: 1H-imidazole / dichloromethane / 6 h / 0 - 20 °C

2.1: phosphonite ligand; tris(dibenzylideneacetone)diplatinum⁽⁰⁾; bis(pinacol)diborane / tetrahydrofuran / 12 h / 60 °C

2.2: 4 h / 0 - 20 °C

3.1: sodium hydrogencarbonate; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; potassium bromide; sodium hypochlorite / dichloromethane; water / 0.5 h / 0 °C / Inert atmosphere

4.1: sodium hydride / tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere

4.2: 3 h / -78 - 20 °C / Inert atmosphere

5.1: copper(l) iodide / tetrahydrofuran / -78 °C

With 1H-imidazole; sodium hypochlorite; copper(l) iodide; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; tris(dibenzylideneacetone)diplatinum⁽⁰⁾; phosphonite ligand; sodium hydride; sodium hydrogencarbonate; bis(pinacol)diborane; potassium bromide; In tetrahydrofuran; dichloromethane; water; 4.1: |Wittig Olefination / 4.2: |Wittig Olefination;
DOI:10.1016/j.tet.2012.11.077