methyl 2-[(3-fluorophenyl)amino]-3-{[(methoxycarbonyl)amino]imino}butanoate

Base Information

Chemical Name:methyl 2-[(3-fluorophenyl)amino]-3-{[(methoxycarbonyl)amino]imino}butanoate
CAS No.:99406-20-9
Molecular Formula:C₁₃H₁₆FN₃O₄
Molecular Weight:297.286
Hs Code.:

Synonyms:methyl 2-[(3-fluorophenyl)amino]-3-{[(methoxycarbonyl)amino]imino}butanoate

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Chemical Property of methyl 2-[(3-fluorophenyl)amino]-3-{[(methoxycarbonyl)amino]imino}butanoate

Chemical Property:

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Technology Process of methyl 2-[(3-fluorophenyl)amino]-3-{[(methoxycarbonyl)amino]imino}butanoate

There total 3 articles about methyl 2-[(3-fluorophenyl)amino]-3-{[(methoxycarbonyl)amino]imino}butanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 372-19-0
meta-fluoroaniline

: 63160-33-8
methyl 3-[[(methoxycarbonyl)imino]amino]but-2-enoate

: 99406-20-9
methyl 2-[(3-fluorophenyl)amino]-3-{[(methoxycarbonyl)amino]imino}butanoate

Guidance literature:: In tetrahydrofuran; at 20 ℃; for 16h;

Reference yield:

: 4755-81-1,935731-92-3
methyl 2-chloroacetoacetate

: 99406-20-9
methyl 2-[(3-fluorophenyl)amino]-3-{[(methoxycarbonyl)amino]imino}butanoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: diethyl ether / 4 h

1.2: 2.5 h

2.1: tetrahydrofuran / 16 h / 20 °C

In tetrahydrofuran; diethyl ether;

Reference yield:

: 63160-32-7
2-Chloro-3-(methoxycarbonyl-hydrazono)-butyric acid methyl ester

: 99406-20-9
methyl 2-[(3-fluorophenyl)amino]-3-{[(methoxycarbonyl)amino]imino}butanoate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydrogencarbonate / diethyl ether; water / 2.5 h

2: tetrahydrofuran / 16 h / 20 °C

With sodium hydrogencarbonate; In tetrahydrofuran; diethyl ether; water;