N-[2-ethoxythiocarbonylsulfanyl-4-phenoxycarbonylbutyl]-4-fluorobenzenesulfonamide

Base Information

Chemical Name:N-[2-ethoxythiocarbonylsulfanyl-4-phenoxycarbonylbutyl]-4-fluorobenzenesulfonamide
CAS No.:946076-63-7
Molecular Formula:C₂₀H₂₂FNO₅S₃
Molecular Weight:471.595
Hs Code.:

Synonyms:N-[2-ethoxythiocarbonylsulfanyl-4-phenoxycarbonylbutyl]-4-fluorobenzenesulfonamide

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Chemical Property of N-[2-ethoxythiocarbonylsulfanyl-4-phenoxycarbonylbutyl]-4-fluorobenzenesulfonamide

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Technology Process of N-[2-ethoxythiocarbonylsulfanyl-4-phenoxycarbonylbutyl]-4-fluorobenzenesulfonamide

There total 1 articles about N-[2-ethoxythiocarbonylsulfanyl-4-phenoxycarbonylbutyl]-4-fluorobenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

: 946076-28-4
dithiocarbonic acid O-ethyl ester S-phenoxycarbonylmethyl ester

: 66898-23-5
N-allyl-4-fluorobenzenesulfonamide

: 946076-63-7
N-[2-ethoxythiocarbonylsulfanyl-4-phenoxycarbonylbutyl]-4-fluorobenzenesulfonamide

Guidance literature:: With dilauryl peroxide; In 1,2-dichloro-ethane; Heating;
DOI:10.1016/j.tet.2007.04.091

Reference yield: 84.0%

: 946076-63-7
N-[2-ethoxythiocarbonylsulfanyl-4-phenoxycarbonylbutyl]-4-fluorobenzenesulfonamide

: 75-36-5
acetyl chloride

: 946076-36-4
N-acetyl-N-[2-ethoxythiocarbonylsulfanyl-4-phenoxycarbonylbutyl]-4-fluorobenzenesulfonamide

Guidance literature:: With dmap; In dichloromethane; at 0 - 20 ℃; for 2h;
DOI:10.1016/j.tet.2007.04.091

Reference yield:

: 946076-63-7
N-[2-ethoxythiocarbonylsulfanyl-4-phenoxycarbonylbutyl]-4-fluorobenzenesulfonamide

: N-[2-(4-fluorophenyl)-4-phenoxycarbonylbutyl]acetamide

Guidance literature:: Multi-step reaction with 2 steps

1: 84 percent / DMAP / CH₂Cl₂ / 2 h / 0 - 20 °C

2: 47 percent / lauroyl peroxide / propan-2-ol; 1,2-dichloro-ethane / Heating

With dmap; dilauryl peroxide; In dichloromethane; 1,2-dichloro-ethane; isopropyl alcohol;
DOI:10.1016/j.tet.2007.04.091