C₂₂H₂₅NO₃

Base Information

Chemical Name:C₂₂H₂₅NO₃
CAS No.:1613157-89-3
Molecular Formula:C₂₂H₂₅NO₃
Molecular Weight:351.445
Hs Code.:

C<sub>22</sub>H<sub>25</sub>NO<sub>3</sub>

Synonyms:C₂₂H₂₅NO₃

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Chemical Property of C₂₂H₂₅NO₃

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Technology Process of C₂₂H₂₅NO₃

There total 8 articles about C₂₂H₂₅NO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 1613157-83-7
(1R,3S,5S)-3-methyl-8-oxa-6-azabicyclo[3.2.1]octane hydrochloride

: 114772-38-2
Methyl 4'-(bromomethyl)biphenyl-2-carboxylate

: 1613157-89-3
C₂₂H₂₅NO₃

Guidance literature:: With triethylamine; In acetonitrile; at 20 ℃; for 12h; Inert atmosphere;
DOI:10.1016/j.bmc.2014.04.040

Reference yield:

: 1613157-78-0
C₁₄H₂₅NO₄

: 1613157-89-3
C₂₂H₂₅NO₃

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium hexamethyldisilazane / tetrahydrofuran / 1 h / 0 °C / Inert atmosphere

1.2: 2 h / 0 °C / Inert atmosphere

2.1: 9-bora-bicyclo[3.3.1]nonane / tetrahydrofuran / 2 h / 0 - 20 °C / Inert atmosphere

2.2: 1 h / 0 - 20 °C

3.1: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 0.5 h / 20 °C / Molecular sieve; Inert atmosphere

4.1: acetic acid / water / 18 h / 60 °C

5.1: hydrogenchloride / ethyl acetate / 0.5 h / 20 °C / Inert atmosphere

6.1: triethylamine / acetonitrile / 12 h / 20 °C / Inert atmosphere

With hydrogenchloride; tetrapropylammonium perruthennate; sodium hexamethyldisilazane; acetic acid; 4-methylmorpholine N-oxide; triethylamine; 9-bora-bicyclo[3.3.1]nonane; In tetrahydrofuran; dichloromethane; water; ethyl acetate; acetonitrile; 1.1: |Wittig Olefination / 1.2: |Wittig Olefination;
DOI:10.1016/j.bmc.2014.04.040

Reference yield:

: 1613157-80-4
tert-butyl (R)-5-((R)-4-hydroxy-2-methylbutyl)-2,2-dimethyloxazolidine-3-carboxylate

: 1613157-89-3
C₂₂H₂₅NO₃

Guidance literature:: Multi-step reaction with 4 steps

1: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 0.5 h / 20 °C / Molecular sieve; Inert atmosphere

2: acetic acid / water / 18 h / 60 °C

3: hydrogenchloride / ethyl acetate / 0.5 h / 20 °C / Inert atmosphere

4: triethylamine / acetonitrile / 12 h / 20 °C / Inert atmosphere

With hydrogenchloride; tetrapropylammonium perruthennate; acetic acid; 4-methylmorpholine N-oxide; triethylamine; In dichloromethane; water; ethyl acetate; acetonitrile;
DOI:10.1016/j.bmc.2014.04.040