3-acetamido-2,6-anhydro-4,5,7-tri-O-benzyl-3-deoxy-1-hydroxy-D-glycero-L-gluco-heptitol

Base Information

Chemical Name:3-acetamido-2,6-anhydro-4,5,7-tri-O-benzyl-3-deoxy-1-hydroxy-D-glycero-L-gluco-heptitol
CAS No.:260551-12-0
Molecular Formula:C₃₀H₃₅NO₆
Molecular Weight:505.611
Hs Code.:

Synonyms:3-acetamido-2,6-anhydro-4,5,7-tri-O-benzyl-3-deoxy-1-hydroxy-D-glycero-L-gluco-heptitol

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Chemical Property of 3-acetamido-2,6-anhydro-4,5,7-tri-O-benzyl-3-deoxy-1-hydroxy-D-glycero-L-gluco-heptitol

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Technology Process of 3-acetamido-2,6-anhydro-4,5,7-tri-O-benzyl-3-deoxy-1-hydroxy-D-glycero-L-gluco-heptitol

There total 4 articles about 3-acetamido-2,6-anhydro-4,5,7-tri-O-benzyl-3-deoxy-1-hydroxy-D-glycero-L-gluco-heptitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 260551-10-8
3-acetamido-2,6-anhydro-4,5,7-tri-O-benzyl-3-deoxy-D-glycero-L-gluco-heptonic acid methyl ester

: 260551-12-0
3-acetamido-2,6-anhydro-4,5,7-tri-O-benzyl-3-deoxy-1-hydroxy-D-glycero-L-gluco-heptitol

Guidance literature:: With sodium tetrahydroborate; In tetrahydrofuran; ethanol; at 0 - 20 ℃;
DOI:10.1021/jo990766l

Reference yield:

: 4171-72-6,4171-79-3,121123-45-3
2-acetamido-2-deoxy-3,4,6-tri-O-benzyl-D-galactopyranose

: 260551-12-0
3-acetamido-2,6-anhydro-4,5,7-tri-O-benzyl-3-deoxy-1-hydroxy-D-glycero-L-gluco-heptitol

Guidance literature:: Multi-step reaction with 4 steps

1: SOCl₂ / toluene; CHCl₃ / 0.5 h

2: 1.24 g / BuLi; lithium naphthalenide / tetrahydrofuran / 1 h / -78 °C

3: 97 percent / CsCO₃ / dimethylformamide / 14 h

4: 71 percent / NaBH₄ / ethanol; tetrahydrofuran / 0 - 20 °C

With sodium tetrahydroborate; n-butyllithium; thionyl chloride; naphthalen-1-yl-lithium; In tetrahydrofuran; ethanol; chloroform; N,N-dimethyl-formamide; toluene; 1: Substitution / 2: Carboxylation / 3: Methylation / 4: Reduction;
DOI:10.1021/jo990766l

Reference yield:

: 201864-30-4
3-acetamido-2,6-anhydro-4,5,7-tri-O-benzyl-3-deoxy-D-glycero-L-gluco-heptonic acid

: 260551-12-0
3-acetamido-2,6-anhydro-4,5,7-tri-O-benzyl-3-deoxy-1-hydroxy-D-glycero-L-gluco-heptitol

Guidance literature:: Multi-step reaction with 2 steps

1: 97 percent / CsCO₃ / dimethylformamide / 14 h

2: 71 percent / NaBH₄ / ethanol; tetrahydrofuran / 0 - 20 °C

With sodium tetrahydroborate; In tetrahydrofuran; ethanol; N,N-dimethyl-formamide; 1: Methylation / 2: Reduction;
DOI:10.1021/jo990766l