{4-[4-(3-aminopropoxy)-3,5-diiodophenoxy]-3,5-diiodophenyl}acetic acid

Base Information

Chemical Name:{4-[4-(3-aminopropoxy)-3,5-diiodophenoxy]-3,5-diiodophenyl}acetic acid
CAS No.:1300559-77-6
Molecular Formula:C₁₇H₁₅I₄NO₄
Molecular Weight:804.928
Hs Code.:

Synonyms:{4-[4-(3-aminopropoxy)-3,5-diiodophenoxy]-3,5-diiodophenyl}acetic acid

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Chemical Property of {4-[4-(3-aminopropoxy)-3,5-diiodophenoxy]-3,5-diiodophenyl}acetic acid

Chemical Property:

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Technology Process of {4-[4-(3-aminopropoxy)-3,5-diiodophenoxy]-3,5-diiodophenyl}acetic acid

There total 11 articles about {4-[4-(3-aminopropoxy)-3,5-diiodophenoxy]-3,5-diiodophenyl}acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1300857-63-9
C₁₈H₁₇I₄NO₄

: 1300559-77-6
{4-[4-(3-aminopropoxy)-3,5-diiodophenoxy]-3,5-diiodophenyl}acetic acid

Guidance literature:: C₁₈H₁₇I₄NO₄; With water; lithium hydroxide;

With hydrogenchloride; In water;

Reference yield:

: 83799-60-4
(4-hydroxy-3,5-dinitro-phenyl)-acetic acid ethyl ester

: 1300559-77-6
{4-[4-(3-aminopropoxy)-3,5-diiodophenoxy]-3,5-diiodophenyl}acetic acid

Guidance literature:: Multi-step reaction with 8 steps

1.1: pyridine; p-toluenesulfonyl chloride / 0.5 h / 95 - 100 °C

1.2: 2 h / 125 °C / Inert atmosphere

2.1: hydrogen / 5% Pd-CaCO3 / ethanol

3.1: sodium nitrite; sulfuric acid; acetic acid / 1.75 h / 0 °C

3.2: 1 h / 20 °C

4.1: phosphorus; hydrogen iodide; acetic acid / 1 h / Reflux

5.1: iodine; ammonia / methanol

6.1: thionyl chloride / 48 h / Reflux

7.1: triethylamine / cyclopentyl methyl ether / 3 h / Reflux

8.1: water; lithium hydroxide

With pyridine; phosphorus; thionyl chloride; sulfuric acid; ammonia; water; hydrogen iodide; hydrogen; iodine; acetic acid; triethylamine; p-toluenesulfonyl chloride; lithium hydroxide; sodium nitrite; 5% Pd-CaCO3; In methanol; ethanol; cyclopentyl methyl ether;

Reference yield:

: 861065-72-7
[4-(4-methoxy-phenoxy)-3,5-dinitro-phenyl]-acetic acid ethyl ester

: 1300559-77-6
{4-[4-(3-aminopropoxy)-3,5-diiodophenoxy]-3,5-diiodophenyl}acetic acid

Guidance literature:: Multi-step reaction with 7 steps

1.1: hydrogen / 5% Pd-CaCO3 / ethanol

2.1: sodium nitrite; sulfuric acid; acetic acid / 1.75 h / 0 °C

2.2: 1 h / 20 °C

3.1: phosphorus; hydrogen iodide; acetic acid / 1 h / Reflux

4.1: iodine; ammonia / methanol

5.1: thionyl chloride / 48 h / Reflux

6.1: triethylamine / cyclopentyl methyl ether / 3 h / Reflux

7.1: water; lithium hydroxide

With phosphorus; thionyl chloride; sulfuric acid; ammonia; water; hydrogen iodide; hydrogen; iodine; acetic acid; triethylamine; lithium hydroxide; sodium nitrite; 5% Pd-CaCO3; In methanol; ethanol; cyclopentyl methyl ether;