4-((benzyl(3-(1,3-dioxoisoindolin-2-yl)propyl)amino)methyl)-N'-phenylbenzohydrazide

Base Information

Chemical Name:4-((benzyl(3-(1,3-dioxoisoindolin-2-yl)propyl)amino)methyl)-N'-phenylbenzohydrazide
CAS No.:1059145-19-5
Molecular Formula:C₃₂H₃₀N₄O₃
Molecular Weight:518.615
Hs Code.:

Synonyms:4-((benzyl(3-(1,3-dioxoisoindolin-2-yl)propyl)amino)methyl)-N'-phenylbenzohydrazide

Suppliers and Price of 4-((benzyl(3-(1,3-dioxoisoindolin-2-yl)propyl)amino)methyl)-N'-phenylbenzohydrazide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 4-((benzyl(3-(1,3-dioxoisoindolin-2-yl)propyl)amino)methyl)-N'-phenylbenzohydrazide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 4-((benzyl(3-(1,3-dioxoisoindolin-2-yl)propyl)amino)methyl)-N'-phenylbenzohydrazide

There total 5 articles about 4-((benzyl(3-(1,3-dioxoisoindolin-2-yl)propyl)amino)methyl)-N'-phenylbenzohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100-46-9
benzylamine

: 1059145-19-5
4-((benzyl(3-(1,3-dioxoisoindolin-2-yl)propyl)amino)methyl)-N'-phenylbenzohydrazide

Guidance literature:: Multi-step reaction with 3 steps

1.1: acetic acid / methanol; 1,2-dichloro-ethane / 0.25 h / 20 °C

1.2: 16 h / 60 °C

2.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 0.25 h / 20 °C

2.2: 17 h / 20 °C

3.1: N-ethyl-N,N-diisopropylamine; sodium iodide / acetonitrile / 48 h / Heating / reflux

With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; sodium iodide; acetic acid; In methanol; 1,2-dichloro-ethane; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 619-66-9
4-Carboxybenzaldehyde

: 1059145-19-5
4-((benzyl(3-(1,3-dioxoisoindolin-2-yl)propyl)amino)methyl)-N'-phenylbenzohydrazide

Guidance literature:: Multi-step reaction with 3 steps

1.1: acetic acid / methanol; 1,2-dichloro-ethane / 0.25 h / 20 °C

1.2: 16 h / 60 °C

2.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 0.25 h / 20 °C

2.2: 17 h / 20 °C

3.1: N-ethyl-N,N-diisopropylamine; sodium iodide / acetonitrile / 48 h / Heating / reflux

With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; sodium iodide; acetic acid; In methanol; 1,2-dichloro-ethane; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 193821-09-9
N-benzyl-(4-methoxycarbonylphenyl)methanimine

: 1059145-19-5
4-((benzyl(3-(1,3-dioxoisoindolin-2-yl)propyl)amino)methyl)-N'-phenylbenzohydrazide

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium tetrahydroborate / methanol / 4 h / 0 - 20 °C

2.1: lithium hydroxide; water / tetrahydrofuran / 17 h / 70 °C

3.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 0.25 h / 20 °C

3.2: 17 h / 20 °C

4.1: N-ethyl-N,N-diisopropylamine; sodium iodide / acetonitrile / 48 h / Heating / reflux

With lithium hydroxide; sodium tetrahydroborate; water; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; sodium iodide; In tetrahydrofuran; methanol; N,N-dimethyl-formamide; acetonitrile;