(S)-3-Methyl-2-[methyl-(toluene-4-sulfonyl)-amino]-butyric acid; compound with dicyclohexyl-amine

Base Information

Chemical Name:(S)-3-Methyl-2-[methyl-(toluene-4-sulfonyl)-amino]-butyric acid; compound with dicyclohexyl-amine
CAS No.:60522-11-4
Molecular Formula:C₁₂H₂₃N*C₁₃H₁₉NO₄S
Molecular Weight:466.685
Hs Code.:

Synonyms:(S)-3-Methyl-2-[methyl-(toluene-4-sulfonyl)-amino]-butyric acid; compound with dicyclohexyl-amine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-3-Methyl-2-[methyl-(toluene-4-sulfonyl)-amino]-butyric acid; compound with dicyclohexyl-amine

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Technology Process of (S)-3-Methyl-2-[methyl-(toluene-4-sulfonyl)-amino]-butyric acid; compound with dicyclohexyl-amine

There total 2 articles about (S)-3-Methyl-2-[methyl-(toluene-4-sulfonyl)-amino]-butyric acid; compound with dicyclohexyl-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 60522-09-0
(S)-3-Methyl-2-[methyl-(toluene-4-sulfonyl)-amino]-butyric acid tert-butyl ester

: 101-83-7
N-cyclohexyl-cyclohexanamine

: 60522-11-4
(S)-3-Methyl-2-[methyl-(toluene-4-sulfonyl)-amino]-butyric acid; compound with dicyclohexyl-amine

Guidance literature:: With trifluoroacetic acid; for 2h;

Reference yield:

: 60522-08-9
tert-butyl 3-methyl-2-(4-methylphenylsulfonamido)butanoate

: 60522-11-4
(S)-3-Methyl-2-[methyl-(toluene-4-sulfonyl)-amino]-butyric acid; compound with dicyclohexyl-amine

Guidance literature:: Multi-step reaction with 2 steps

1: 97 percent / NaOH / H₂O / 4 h / Ambient temperature; detergent

2: 94 percent / CF₃COOH / 2 h

With sodium hydroxide; trifluoroacetic acid; In water;

Reference yield: 90.0%

: 593-51-1
methylamine hydrochloride

: 60522-11-4
(S)-3-Methyl-2-[methyl-(toluene-4-sulfonyl)-amino]-butyric acid; compound with dicyclohexyl-amine

: 124312-59-0
(S)-3,N-Dimethyl-2-[methyl-(toluene-4-sulfonyl)-amino]-butyramide

Guidance literature:: With benzotriazol-1-ol; dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide; 1. -12 deg C, 30 min; 2. 0 deg C, 2 h; 3. 5 deg c, 18 h;