(4S)-4-[(1R)-1-(tert-butyldiphenylsilyloxy)-hexadec-2-enyl]-2-chloro-2-oxo-[1,3,2]-oxazaphospholidine

Base Information

Chemical Name:(4S)-4-[(1R)-1-(tert-butyldiphenylsilyloxy)-hexadec-2-enyl]-2-chloro-2-oxo-[1,3,2]-oxazaphospholidine
CAS No.:860021-45-0
Molecular Formula:C₃₄H₅₃ClNO₃PSi
Molecular Weight:618.312
Hs Code.:

Synonyms:(4S)-4-[(1R)-1-(tert-butyldiphenylsilyloxy)-hexadec-2-enyl]-2-chloro-2-oxo-[1,3,2]-oxazaphospholidine

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Chemical Property of (4S)-4-[(1R)-1-(tert-butyldiphenylsilyloxy)-hexadec-2-enyl]-2-chloro-2-oxo-[1,3,2]-oxazaphospholidine

Chemical Property:

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MSDS Files:: SDS file from LookChem

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Technology Process of (4S)-4-[(1R)-1-(tert-butyldiphenylsilyloxy)-hexadec-2-enyl]-2-chloro-2-oxo-[1,3,2]-oxazaphospholidine

There total 1 articles about (4S)-4-[(1R)-1-(tert-butyldiphenylsilyloxy)-hexadec-2-enyl]-2-chloro-2-oxo-[1,3,2]-oxazaphospholidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 867062-44-0
3-O-tert-butyldiphenylsilyl-D-erythro-sphingosine

: 860021-45-0
(4S)-4-[(1R)-1-(tert-butyldiphenylsilyloxy)-hexadec-2-enyl]-2-chloro-2-oxo-[1,3,2]-oxazaphospholidine

Guidance literature:: With triethylamine; trichlorophosphate; In hexane; dichloromethane; at -20 - -10 ℃;

Reference yield: 31.0%

: 860021-45-0
(4S)-4-[(1R)-1-(tert-butyldiphenylsilyloxy)-hexadec-2-enyl]-2-chloro-2-oxo-[1,3,2]-oxazaphospholidine

: 55357-38-5
choline tosylate

: 112-67-4
n-hexadecanoyl chloride

: 536-14-1,4846-15-5,13053-57-1,6254-89-3
N-palmitoyl-D-erythro-sphingomyelin

Guidance literature:: (4S)-4-[(1R)-1-(tert-butyldiphenylsilyloxy)-hexadec-2-enyl]-2-chloro-2-oxo-[1,3,2]-oxazaphospholidine; choline tosylate; With triethylamine; In dichloromethane; acetonitrile; at 20 ℃; for 12h;

With hydrogenchloride; water; In tetrahydrofuran;

n-hexadecanoyl chloride; With tetrabutyl ammonium fluoride; more than 3 stages;

Reference yield: 23.0%

: 860021-45-0
(4S)-4-[(1R)-1-(tert-butyldiphenylsilyloxy)-hexadec-2-enyl]-2-chloro-2-oxo-[1,3,2]-oxazaphospholidine

: 55357-38-5
choline tosylate

: 1670-26-4,105615-55-2,82970-80-7
sphingosylphosphorylcholine

Guidance literature:: (4S)-4-[(1R)-1-(tert-butyldiphenylsilyloxy)-hexadec-2-enyl]-2-chloro-2-oxo-[1,3,2]-oxazaphospholidine; choline tosylate; With triethylamine; In dichloromethane; acetonitrile;

With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 45 ℃; for 2h;