(S)-2-((S)-2-Benzyloxycarbonylamino-3-phenyl-propionylamino)-4-methyl-pentanoic acid 2-methoxy-ethyl ester

Base Information

Chemical Name:(S)-2-((S)-2-Benzyloxycarbonylamino-3-phenyl-propionylamino)-4-methyl-pentanoic acid 2-methoxy-ethyl ester
CAS No.:111633-79-5
Molecular Formula:C₂₆H₃₄N₂O₆
Molecular Weight:470.566
Hs Code.:

Synonyms:(S)-2-((S)-2-Benzyloxycarbonylamino-3-phenyl-propionylamino)-4-methyl-pentanoic acid 2-methoxy-ethyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-2-((S)-2-Benzyloxycarbonylamino-3-phenyl-propionylamino)-4-methyl-pentanoic acid 2-methoxy-ethyl ester

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Technology Process of (S)-2-((S)-2-Benzyloxycarbonylamino-3-phenyl-propionylamino)-4-methyl-pentanoic acid 2-methoxy-ethyl ester

There total 2 articles about (S)-2-((S)-2-Benzyloxycarbonylamino-3-phenyl-propionylamino)-4-methyl-pentanoic acid 2-methoxy-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 1161-13-3
N-Cbz-L-Phe

: 2-methoxy ethyl tyrosyl ester hydrochloride

: 111633-79-5
(S)-2-((S)-2-Benzyloxycarbonylamino-3-phenyl-propionylamino)-4-methyl-pentanoic acid 2-methoxy-ethyl ester

Guidance literature:: With triethylamine; dimethylphosphinothioic chloride; In chloroform; for 11h; Ambient temperature;
DOI:10.1246/bcsj.60.267

Reference yield:

: 61-90-5,21675-61-6,25248-98-0,70-45-1
L-leucine

: 111633-79-5
(S)-2-((S)-2-Benzyloxycarbonylamino-3-phenyl-propionylamino)-4-methyl-pentanoic acid 2-methoxy-ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: SOCl₂

2: 62 percent / dimethylphosphinothioic chloride, triethylamine / CHCl₃ / 11 h / Ambient temperature

With thionyl chloride; triethylamine; dimethylphosphinothioic chloride; In chloroform;
DOI:10.1246/bcsj.60.267