diphenylmethylamino-p-methoxy-m-(tert-butyldimethylsilyloxy)phenylacetonitryle

Base Information

Chemical Name:diphenylmethylamino-p-methoxy-m-(tert-butyldimethylsilyloxy)phenylacetonitryle
CAS No.:586413-60-7
Molecular Formula:C₂₈H₃₄N₂O₂Si
Molecular Weight:458.676
Hs Code.:

Synonyms:diphenylmethylamino-p-methoxy-m-(tert-butyldimethylsilyloxy)phenylacetonitryle

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Chemical Property of diphenylmethylamino-p-methoxy-m-(tert-butyldimethylsilyloxy)phenylacetonitryle

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Technology Process of diphenylmethylamino-p-methoxy-m-(tert-butyldimethylsilyloxy)phenylacetonitryle

There total 4 articles about diphenylmethylamino-p-methoxy-m-(tert-butyldimethylsilyloxy)phenylacetonitryle which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 621-59-0
isovanillin

: 586413-60-7
diphenylmethylamino-p-methoxy-m-(tert-butyldimethylsilyloxy)phenylacetonitryle

Guidance literature:: Multi-step reaction with 3 steps

1: 98 percent / imidazole / dimethylformamide / 0.5 h

2: 98 percent / MgSO₄ / benzene / 24 h

3: Ti(O-i-Pr)4; chiral amino acid ligand; isopropanol / toluene / 4 h

With 1H-imidazole; titanium(IV) isopropylate; chiral amino acid ligand; magnesium sulfate; isopropyl alcohol; In N,N-dimethyl-formamide; toluene; benzene;
DOI:10.1021/ja030249r

Reference yield:

: 18162-48-6
tert-butyldimethylsilyl chloride

: 586413-60-7
diphenylmethylamino-p-methoxy-m-(tert-butyldimethylsilyloxy)phenylacetonitryle

Guidance literature:: Multi-step reaction with 3 steps

1: 98 percent / imidazole / dimethylformamide / 0.5 h

2: 98 percent / MgSO₄ / benzene / 24 h

3: Ti(O-i-Pr)4; chiral amino acid ligand; isopropanol / toluene / 4 h

With 1H-imidazole; titanium(IV) isopropylate; chiral amino acid ligand; magnesium sulfate; isopropyl alcohol; In N,N-dimethyl-formamide; toluene; benzene;
DOI:10.1021/ja030249r

Reference yield:

: 97315-18-9
p-methoxy-m-(tert-butyldimethylsilyloxy)-benzaldehyde

: 586413-60-7
diphenylmethylamino-p-methoxy-m-(tert-butyldimethylsilyloxy)phenylacetonitryle

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / MgSO₄ / benzene / 24 h

2: Ti(O-i-Pr)4; chiral amino acid ligand; isopropanol / toluene / 4 h

With titanium(IV) isopropylate; chiral amino acid ligand; magnesium sulfate; isopropyl alcohol; In toluene; benzene;
DOI:10.1021/ja030249r