N-[[1-[(2(S)-acetylmercapto-3-methyl-1-oxobutyl)amino]-1-cyclopentyl]carbonyl]-L-tyrosinemethyl ester

Base Information

Chemical Name:N-[[1-[(2(S)-acetylmercapto-3-methyl-1-oxobutyl)amino]-1-cyclopentyl]carbonyl]-L-tyrosinemethyl ester
CAS No.:169319-29-3
Molecular Formula:C₂₃H₃₂N₂O₆S
Molecular Weight:464.583
Hs Code.:

Synonyms:N-[[1-[(2(S)-acetylmercapto-3-methyl-1-oxobutyl)amino]-1-cyclopentyl]carbonyl]-L-tyrosinemethyl ester

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Chemical Property of N-[[1-[(2(S)-acetylmercapto-3-methyl-1-oxobutyl)amino]-1-cyclopentyl]carbonyl]-L-tyrosinemethyl ester

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Technology Process of N-[[1-[(2(S)-acetylmercapto-3-methyl-1-oxobutyl)amino]-1-cyclopentyl]carbonyl]-L-tyrosinemethyl ester

There total 5 articles about N-[[1-[(2(S)-acetylmercapto-3-methyl-1-oxobutyl)amino]-1-cyclopentyl]carbonyl]-L-tyrosinemethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 35264-09-6
1-(tert-butoxycarbonylamino)cyclopentanecarboxylic acid

: 169319-29-3
N-[[1-[(2(S)-acetylmercapto-3-methyl-1-oxobutyl)amino]-1-cyclopentyl]carbonyl]-L-tyrosinemethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 61 percent / 1,3-dicyclohexylcarbodiimide, 1-hydroxybenzotriazole / CH₂Cl₂

2: HCl / CH₂Cl₂ / 0.25 h

3: Et₃N, 1,3-dicyclohexylcarbodiimide, 1-hydroxy-7-azabenzotriazole / CH₂Cl₂ / 16 h

With hydrogenchloride; 1-hydroxy-7-aza-benzotriazole; benzotriazol-1-ol; triethylamine; dicyclohexyl-carbodiimide; In dichloromethane;
DOI:10.1021/jm960323z

Reference yield:

: 169320-24-5
(S)-2-[(1-tert-Butoxycarbonylamino-cyclopentanecarbonyl)-amino]-3-(4-hydroxy-phenyl)-propionic acid methyl ester

: 169319-29-3
N-[[1-[(2(S)-acetylmercapto-3-methyl-1-oxobutyl)amino]-1-cyclopentyl]carbonyl]-L-tyrosinemethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: HCl / CH₂Cl₂ / 0.25 h

2: Et₃N, 1,3-dicyclohexylcarbodiimide, 1-hydroxy-7-azabenzotriazole / CH₂Cl₂ / 16 h

With hydrogenchloride; 1-hydroxy-7-aza-benzotriazole; triethylamine; dicyclohexyl-carbodiimide; In dichloromethane;
DOI:10.1021/jm960323z

Reference yield:

: (S)-2-[(1-Amino-cyclopentanecarbonyl)-amino]-3-(4-hydroxy-phenyl)-propionic acid methyl ester; hydrochloride

: 149603-80-5
(2S)-2-(acetylthio)-3-methylbutanoic acid

: 169319-29-3
N-[[1-[(2(S)-acetylmercapto-3-methyl-1-oxobutyl)amino]-1-cyclopentyl]carbonyl]-L-tyrosinemethyl ester

Guidance literature:: With 1-hydroxy-7-aza-benzotriazole; triethylamine; dicyclohexyl-carbodiimide; Yield given. Multistep reaction; 1.) CH₂Cl₂, 5 min, 2.) CH₂Cl₂, 16 h;