6-(4-chloro-3-fluorophenyl)-1-(3-(4-chlorophenoxy)propyl)-1,6-dihydro-1,3,5-triazine-2,4-diamine hydrochloride

Base Information

Chemical Name:6-(4-chloro-3-fluorophenyl)-1-(3-(4-chlorophenoxy)propyl)-1,6-dihydro-1,3,5-triazine-2,4-diamine hydrochloride
CAS No.:1266246-56-3
Molecular Formula:C₁₈H₁₈Cl₂FN₅O*ClH
Molecular Weight:446.739
Hs Code.:

Synonyms:6-(4-chloro-3-fluorophenyl)-1-(3-(4-chlorophenoxy)propyl)-1,6-dihydro-1,3,5-triazine-2,4-diamine hydrochloride

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Chemical Property of 6-(4-chloro-3-fluorophenyl)-1-(3-(4-chlorophenoxy)propyl)-1,6-dihydro-1,3,5-triazine-2,4-diamine hydrochloride

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Technology Process of 6-(4-chloro-3-fluorophenyl)-1-(3-(4-chlorophenoxy)propyl)-1,6-dihydro-1,3,5-triazine-2,4-diamine hydrochloride

There total 3 articles about 6-(4-chloro-3-fluorophenyl)-1-(3-(4-chlorophenoxy)propyl)-1,6-dihydro-1,3,5-triazine-2,4-diamine hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 18.0%

: C₁₆H₁₄Cl₂FNO

: 127099-85-8,780722-26-1,461-58-5
N-Cyanoguanidine

: 1266246-56-3
6-(4-chloro-3-fluorophenyl)-1-(3-(4-chlorophenoxy)propyl)-1,6-dihydro-1,3,5-triazine-2,4-diamine hydrochloride

Guidance literature:: C₁₆H₁₄Cl₂FNO; With hydrogenchloride;

N-Cyanoguanidine; In N,N-dimethyl-formamide; at 100 ℃; for 0.5h; Microwave irradiation;
DOI:10.1039/c6ob01350c

Reference yield:

: 50911-60-9
3-(4-chlorophenoxy)propan-1-amine

: 5527-95-7
4-chloro-3-fluorobenzaldehyde

: 1266246-56-3
6-(4-chloro-3-fluorophenyl)-1-(3-(4-chlorophenoxy)propyl)-1,6-dihydro-1,3,5-triazine-2,4-diamine hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1.1: montmorillonite K-10 / 1,4-dioxane / 0.5 h / 100 °C / Microwave irradiation

2.1: hydrogenchloride

2.2: 0.5 h / 100 °C / Microwave irradiation

With hydrogenchloride; In 1,4-dioxane;
DOI:10.1039/c6ob01350c