Technology Process of C39H42N2O6Si
There total 8 articles about C39H42N2O6Si which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C46H56N2O9Si;
With
hydrogenchloride;
In
1,4-dioxane; dichloromethane;
for 1.5h;
With
1,8-diazabicyclo[5.4.0]undec-7-ene;
In
toluene;
at 110 ℃;
for 0.583333h;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: lithium borohydride / tetrahydrofuran / 18 h / 20 °C / Cooling with ice
2.1: phthalimide; triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 20 h / 20 °C / Cooling with ice
2.2: 2 h / 70 °C
3.1: sodium hydrogencarbonate / ethanol; water / 20 h
4.1: hydrogenchloride / dichloromethane; 1,4-dioxane / 1.5 h
4.2: 0.58 h / 110 °C
With
hydrogenchloride; lithium borohydride; phthalimide; di-isopropyl azodicarboxylate; sodium hydrogencarbonate; triphenylphosphine;
In
tetrahydrofuran; 1,4-dioxane; ethanol; dichloromethane; water;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: hydrogen; 10% palladium hydroxide on charcoal / ethanol; acetic acid / 40 h / 38002.6 Torr
2.1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 20 h
3.1: lithium borohydride / tetrahydrofuran / 18 h / 20 °C / Cooling with ice
4.1: phthalimide; triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 20 h / 20 °C / Cooling with ice
4.2: 2 h / 70 °C
5.1: sodium hydrogencarbonate / ethanol; water / 20 h
6.1: hydrogenchloride / dichloromethane; 1,4-dioxane / 1.5 h
6.2: 0.58 h / 110 °C
With
hydrogenchloride; lithium borohydride; phthalimide; di-isopropyl azodicarboxylate; 10% palladium hydroxide on charcoal; hydrogen; sodium hydrogencarbonate; N-ethyl-N,N-diisopropylamine; triphenylphosphine;
In
tetrahydrofuran; 1,4-dioxane; ethanol; dichloromethane; water; acetic acid;