1,6-dihydro-6-imino-1-methyl-4-methylamino-5-phenylazopyrimidine hydriodide

Base Information

Chemical Name:1,6-dihydro-6-imino-1-methyl-4-methylamino-5-phenylazopyrimidine hydriodide
CAS No.:89073-86-9
Molecular Formula:C₁₂H₁₄N₆*HI
Molecular Weight:370.196
Hs Code.:

Synonyms:1,6-dihydro-6-imino-1-methyl-4-methylamino-5-phenylazopyrimidine hydriodide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,6-dihydro-6-imino-1-methyl-4-methylamino-5-phenylazopyrimidine hydriodide

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Technology Process of 1,6-dihydro-6-imino-1-methyl-4-methylamino-5-phenylazopyrimidine hydriodide

There total 4 articles about 1,6-dihydro-6-imino-1-methyl-4-methylamino-5-phenylazopyrimidine hydriodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 83366-39-6
4-amino-6-methylamino-5-phenylazopyrimidine

: 74-88-4
methyl iodide

: 89073-86-9
1,6-dihydro-6-imino-1-methyl-4-methylamino-5-phenylazopyrimidine hydriodide

Guidance literature:: In N,N-dimethyl-formamide; for 2h; Ambient temperature;
DOI:10.1248/cpb.31.3454

Reference yield:

: 6017-21-6
benzeneazomalononitrile

: 89073-86-9
1,6-dihydro-6-imino-1-methyl-4-methylamino-5-phenylazopyrimidine hydriodide

Guidance literature:: Multi-step reaction with 2 steps

1: 28 percent / HCl / 5 h / 150 °C

2: 52 percent / dimethylformamide / 2 h / Ambient temperature

With hydrogenchloride; In N,N-dimethyl-formamide;
DOI:10.1248/cpb.31.3454

Reference yield:

: 54288-02-7,1321895-41-3
4,6-diamino-5-phenylazopyrimidine

: 89073-86-9
1,6-dihydro-6-imino-1-methyl-4-methylamino-5-phenylazopyrimidine hydriodide

Guidance literature:: Multi-step reaction with 3 steps

1: 38 percent / dimethylformamide / 2 h / Ambient temperature

2: 89 percent / (CH₃)2NH-MeOH / 12 h / Ambient temperature

3: 52 percent / dimethylformamide / 2 h / Ambient temperature

With methanol; dimethyl amine; In N,N-dimethyl-formamide;
DOI:10.1248/cpb.31.3454