7-[(7-{[5-(4-chlorophenyl)-1-(2,4-dichlorophenyl)-4-methyl-1H-pyrazol-3-yl]formamido}heptyl)(methyl)amino]heptanoic acid

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Chemical Name:7-[(7-{[5-(4-chlorophenyl)-1-(2,4-dichlorophenyl)-4-methyl-1H-pyrazol-3-yl]formamido}heptyl)(methyl)amino]heptanoic acid
CAS No.:1584647-16-4
Molecular Formula:C₃₂H₄₁Cl₃N₄O₃
Molecular Weight:636.062
Hs Code.:

Synonyms:7-[(7-{[5-(4-chlorophenyl)-1-(2,4-dichlorophenyl)-4-methyl-1H-pyrazol-3-yl]formamido}heptyl)(methyl)amino]heptanoic acid

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Chemical Property of 7-[(7-{[5-(4-chlorophenyl)-1-(2,4-dichlorophenyl)-4-methyl-1H-pyrazol-3-yl]formamido}heptyl)(methyl)amino]heptanoic acid

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Technology Process of 7-[(7-{[5-(4-chlorophenyl)-1-(2,4-dichlorophenyl)-4-methyl-1H-pyrazol-3-yl]formamido}heptyl)(methyl)amino]heptanoic acid

There total 4 articles about 7-[(7-{[5-(4-chlorophenyl)-1-(2,4-dichlorophenyl)-4-methyl-1H-pyrazol-3-yl]formamido}heptyl)(methyl)amino]heptanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1584647-24-4
C₃₄H₄₅Cl₃N₄O₃

: 1584647-16-4
7-[(7-{[5-(4-chlorophenyl)-1-(2,4-dichlorophenyl)-4-methyl-1H-pyrazol-3-yl]formamido}heptyl)(methyl)amino]heptanoic acid

Guidance literature:: With water; sodium hydroxide; In ethanol; at 20 ℃;
DOI:10.1021/ml4004759

Reference yield:

: 1338604-42-4
N-(7-aminoheptyl)-5-(4-chlorophenyl)-1-(2,4-dichlorophenyl)-4-methyl-1H-pyrazole-3-carboxamide

: 1584647-16-4
7-[(7-{[5-(4-chlorophenyl)-1-(2,4-dichlorophenyl)-4-methyl-1H-pyrazol-3-yl]formamido}heptyl)(methyl)amino]heptanoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / toluene / Reflux

2: sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane; water / 2 h / 20 °C

3: sodium hydroxide; water / ethanol / 20 °C

With water; sodium tris(acetoxy)borohydride; triethylamine; sodium hydroxide; In ethanol; water; 1,2-dichloro-ethane; toluene;
DOI:10.1021/ml4004759

Reference yield:

: 646-19-5
heptane-1,7-diamine

: 1584647-16-4
7-[(7-{[5-(4-chlorophenyl)-1-(2,4-dichlorophenyl)-4-methyl-1H-pyrazol-3-yl]formamido}heptyl)(methyl)amino]heptanoic acid

Guidance literature:: Multi-step reaction with 4 steps

1: (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate / tetrahydrofuran / 20 °C / Inert atmosphere

2: triethylamine / toluene / Reflux

3: sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane; water / 2 h / 20 °C

4: sodium hydroxide; water / ethanol / 20 °C

With water; sodium tris(acetoxy)borohydride; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; triethylamine; sodium hydroxide; In tetrahydrofuran; ethanol; water; 1,2-dichloro-ethane; toluene;
DOI:10.1021/ml4004759