2-isopropyl-6-[2-(7-methyl-1,4-dithiaspiro[4.5]dec-6-en-6-yl)ethyl]phenylmethyl ether

Base Information

Chemical Name:2-isopropyl-6-[2-(7-methyl-1,4-dithiaspiro[4.5]dec-6-en-6-yl)ethyl]phenylmethyl ether
CAS No.:1245920-26-6
Molecular Formula:C₂₁H₃₀OS₂
Molecular Weight:362.601
Hs Code.:

Synonyms:2-isopropyl-6-[2-(7-methyl-1,4-dithiaspiro[4.5]dec-6-en-6-yl)ethyl]phenylmethyl ether

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Chemical Property of 2-isopropyl-6-[2-(7-methyl-1,4-dithiaspiro[4.5]dec-6-en-6-yl)ethyl]phenylmethyl ether

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Technology Process of 2-isopropyl-6-[2-(7-methyl-1,4-dithiaspiro[4.5]dec-6-en-6-yl)ethyl]phenylmethyl ether

There total 2 articles about 2-isopropyl-6-[2-(7-methyl-1,4-dithiaspiro[4.5]dec-6-en-6-yl)ethyl]phenylmethyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 1245920-23-3
2-[2-(3-isopropyl-2-methoxyphenyl)ethyl]-3-methylcyclohex-2-en-1-one

: 540-63-6
ethane-1,2-dithiol

: 1245920-26-6
2-isopropyl-6-[2-(7-methyl-1,4-dithiaspiro[4.5]dec-6-en-6-yl)ethyl]phenylmethyl ether

Guidance literature:: With indium(III) triflate; In dichloromethane; for 30h; Inert atmosphere;
DOI:10.1039/c0cc00250j

Reference yield:

: 1245920-27-7
2-isopropyl-6-[2-(8-methyl-1,5-dithiaspiro[5.5]undec-7-en-7-yl)ethyl]phenyl methyl ether

: 1245920-26-6
2-isopropyl-6-[2-(7-methyl-1,4-dithiaspiro[4.5]dec-6-en-6-yl)ethyl]phenylmethyl ether

Guidance literature:: Multi-step reaction with 2 steps

1: trimethylsilyl trifluoromethanesulfonate / 1,2-dichloro-ethane / 16 h / 20 °C / Inert atmosphere

2: indium(III) trifluoromethanesulfonate / dichloromethane / 30 h / 20 °C / Inert atmosphere

With trimethylsilyl trifluoromethanesulfonate; indium(III) trifluoromethanesulfonate; In dichloromethane; 1,2-dichloro-ethane;
DOI:10.1021/jo2001116