spiro[3-(4-methoxybenzylidene)-2-methylidenecyclohexane-1,2'-(5-(4-methoxybenzylidene)-1,3-bis(4-methoxyphenyl)-1,2,3,4,5,6,7,8-octahydronaphthalene)]

Base Information

Chemical Name:spiro[3-(4-methoxybenzylidene)-2-methylidenecyclohexane-1,2'-(5-(4-methoxybenzylidene)-1,3-bis(4-methoxyphenyl)-1,2,3,4,5,6,7,8-octahydronaphthalene)]
CAS No.:564441-87-8
Molecular Formula:C₄₆H₄₈O₄
Molecular Weight:664.885
Hs Code.:

spiro[3-(4-methoxybenzylidene)-2-methylidenecyclohexane-1,2'-(5-(4-methoxybenzylidene)-1,3-bis(4-methoxyphenyl)-1,2,3,4,5,6,7,8-octahydronaphthalene)]

Synonyms:spiro[3-(4-methoxybenzylidene)-2-methylidenecyclohexane-1,2'-(5-(4-methoxybenzylidene)-1,3-bis(4-methoxyphenyl)-1,2,3,4,5,6,7,8-octahydronaphthalene)]

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Chemical Property of spiro[3-(4-methoxybenzylidene)-2-methylidenecyclohexane-1,2'-(5-(4-methoxybenzylidene)-1,3-bis(4-methoxyphenyl)-1,2,3,4,5,6,7,8-octahydronaphthalene)]

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Technology Process of spiro[3-(4-methoxybenzylidene)-2-methylidenecyclohexane-1,2'-(5-(4-methoxybenzylidene)-1,3-bis(4-methoxyphenyl)-1,2,3,4,5,6,7,8-octahydronaphthalene)]

There total 4 articles about spiro[3-(4-methoxybenzylidene)-2-methylidenecyclohexane-1,2'-(5-(4-methoxybenzylidene)-1,3-bis(4-methoxyphenyl)-1,2,3,4,5,6,7,8-octahydronaphthalene)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 501687-39-4
1-methyl-2,6-bis(4-methoxyphenylmethylidene)cyclohexanol

: 564441-87-8
spiro[3-(4-methoxybenzylidene)-2-methylidenecyclohexane-1,2'-(5-(4-methoxybenzylidene)-1,3-bis(4-methoxyphenyl)-1,2,3,4,5,6,7,8-octahydronaphthalene)]

Guidance literature:: With acetic acid; trifluoroacetic acid; for 1h; Heating;
DOI:10.1039/b210890a

Reference yield:

: 6275-32-7,62085-71-6
(2E,6E)-2,6-bis(4-methoxybenzylidene)cyclohexanone

: 564441-87-8
spiro[3-(4-methoxybenzylidene)-2-methylidenecyclohexane-1,2'-(5-(4-methoxybenzylidene)-1,3-bis(4-methoxyphenyl)-1,2,3,4,5,6,7,8-octahydronaphthalene)]

Guidance literature:: Multi-step reaction with 2 steps

1: 72 percent / benzene; diethyl ether / 0.5 h

2: 67 percent / CF₃COOH; glacial acetic acid / 1 h / Heating

With acetic acid; trifluoroacetic acid; In diethyl ether; benzene;
DOI:10.1039/b210890a

Reference yield:

: 108-94-1,11119-77-0,9003-41-2,9075-99-4
cyclohexanone

: 564441-87-8
spiro[3-(4-methoxybenzylidene)-2-methylidenecyclohexane-1,2'-(5-(4-methoxybenzylidene)-1,3-bis(4-methoxyphenyl)-1,2,3,4,5,6,7,8-octahydronaphthalene)]

Guidance literature:: Multi-step reaction with 3 steps

1: 67 percent / aq. ethanol / alkaline solution

2: 72 percent / benzene; diethyl ether / 0.5 h

3: 67 percent / CF₃COOH; glacial acetic acid / 1 h / Heating

With acetic acid; trifluoroacetic acid; In diethyl ether; ethanol; benzene;
DOI:10.1039/b210890a