Acetic acid (1S,6R)-3-(3,4-dimethoxy-phenyl)-6-methoxymethoxy-cyclohex-2-enyl ester

Base Information

Chemical Name:Acetic acid (1S,6R)-3-(3,4-dimethoxy-phenyl)-6-methoxymethoxy-cyclohex-2-enyl ester
CAS No.:187277-52-7
Molecular Formula:C₁₈H₂₄O₆
Molecular Weight:336.385
Hs Code.:

Synonyms:Acetic acid (1S,6R)-3-(3,4-dimethoxy-phenyl)-6-methoxymethoxy-cyclohex-2-enyl ester

Suppliers and Price of Acetic acid (1S,6R)-3-(3,4-dimethoxy-phenyl)-6-methoxymethoxy-cyclohex-2-enyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Acetic acid (1S,6R)-3-(3,4-dimethoxy-phenyl)-6-methoxymethoxy-cyclohex-2-enyl ester

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Technology Process of Acetic acid (1S,6R)-3-(3,4-dimethoxy-phenyl)-6-methoxymethoxy-cyclohex-2-enyl ester

There total 1 articles about Acetic acid (1S,6R)-3-(3,4-dimethoxy-phenyl)-6-methoxymethoxy-cyclohex-2-enyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 18.0%

: 108-24-7
acetic anhydride

: (R)-3-(3,4-Dimethoxy-phenyl)-6-methoxymethoxy-cyclohex-2-enol

: 187277-51-6
Acetic acid (1R,6R)-3-(3,4-dimethoxy-phenyl)-6-methoxymethoxy-cyclohex-2-enyl ester

: 187277-52-7
Acetic acid (1S,6R)-3-(3,4-dimethoxy-phenyl)-6-methoxymethoxy-cyclohex-2-enyl ester

Guidance literature:: With pyridine; for 12h; Ambient temperature;
DOI:10.1039/a604365h

Reference yield: 100.0%

: 187277-52-7
Acetic acid (1S,6R)-3-(3,4-dimethoxy-phenyl)-6-methoxymethoxy-cyclohex-2-enyl ester

: 156558-40-6
(3S,4R)-1-(3,4-Dimethoxyphenyl)-3-hydroxy-4-(methoxymethoxy)cyclohexene

Guidance literature:: With potassium carbonate; In methanol; for 1h; Ambient temperature;
DOI:10.1039/a604365h

Reference yield:

: 187277-52-7
Acetic acid (1S,6R)-3-(3,4-dimethoxy-phenyl)-6-methoxymethoxy-cyclohex-2-enyl ester

: 156487-80-8
N-<2-<(1R,4R)-1-(3,4-Dimethoxyphenyl)-4-(methoxymethoxy)cyclohex-2-enyl>>ethyl-N-methylamine

Guidance literature:: Multi-step reaction with 5 steps

1: 100 percent / K₂CO₃ / methanol / 1 h / Ambient temperature

2: 1.) PPh₃, benzoic acid, diethyl azodicarboxylate, 2.) K₂CO₃ / 1.) Et₂O, r.t., 30 min, 2.) MeOH, r.t., 2 h

3: 58 percent / molecular sieves 3 Angstroem, propionic acid / 48 h / 130 °C

4: 82 percent / DIBALH / toluene / 0.25 h / -78 °C

5: 61 percent / NaBH₃CN, CH₃NH₂ / methanol / 24 h / Ambient temperature

With 3 A molecular sieve; diisobutylaluminium hydride; sodium cyanoborohydride; potassium carbonate; propionic acid; triphenylphosphine; benzoic acid; methylamine; diethylazodicarboxylate; In methanol; toluene;
DOI:10.1039/a604365h