6-[4-(2-nitroimidazol-1-ylmethyl)-1,2,3-triazol-1-yl]flavonol

Base Information

Chemical Name:6-[4-(2-nitroimidazol-1-ylmethyl)-1,2,3-triazol-1-yl]flavonol
CAS No.:1332713-49-1
Molecular Formula:C₂₁H₁₄N₆O₅
Molecular Weight:430.379
Hs Code.:

Synonyms:6-[4-(2-nitroimidazol-1-ylmethyl)-1,2,3-triazol-1-yl]flavonol

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Chemical Property of 6-[4-(2-nitroimidazol-1-ylmethyl)-1,2,3-triazol-1-yl]flavonol

Chemical Property:

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Technology Process of 6-[4-(2-nitroimidazol-1-ylmethyl)-1,2,3-triazol-1-yl]flavonol

There total 4 articles about 6-[4-(2-nitroimidazol-1-ylmethyl)-1,2,3-triazol-1-yl]flavonol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 1070878-68-0
2-nitro-1-(prop-2-yn-1-yl)-1H-imidazole

: 1332713-52-6
6-azidoflavonol

: 1332713-49-1
6-[4-(2-nitroimidazol-1-ylmethyl)-1,2,3-triazol-1-yl]flavonol

Guidance literature:: With copper(II) sulfate; sodium L-ascorbate; tris[(1-benzyl-1H-1,2,3-triazol-4yl)methyl]amine; In water; dimethyl sulfoxide; at 20 ℃;
DOI:10.1016/j.bmcl.2011.03.040

Reference yield:

: 50-80-6
5-amino-2-hydroxyacetophenone

: 1332713-49-1
6-[4-(2-nitroimidazol-1-ylmethyl)-1,2,3-triazol-1-yl]flavonol

Guidance literature:: Multi-step reaction with 4 steps

1.1: sulfuric acid; sodium nitrite / water / 0.5 h / 0 °C

1.2: 0 - 20 °C

2.1: sodium hydroxide / ethanol; water / 20 °C

3.1: dihydrogen peroxide; sodium hydroxide / ethanol; water / 20 °C / Cooling with ice

4.1: copper(II) sulfate; sodium L-ascorbate; tris[(1-benzyl-1H-1,2,3-triazol-4yl)methyl]amine / water; dimethyl sulfoxide / 20 °C

With sulfuric acid; dihydrogen peroxide; copper(II) sulfate; sodium L-ascorbate; sodium hydroxide; sodium nitrite; tris[(1-benzyl-1H-1,2,3-triazol-4yl)methyl]amine; In ethanol; water; dimethyl sulfoxide; 2.1: Claisen-Schmidt condensation / 3.1: Algar-Flynn-Olyamada (AFO) reaction;
DOI:10.1016/j.bmcl.2011.03.040

Reference yield:

: 100-52-7
benzaldehyde

: 1332713-49-1
6-[4-(2-nitroimidazol-1-ylmethyl)-1,2,3-triazol-1-yl]flavonol

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydroxide / ethanol; water / 20 °C

2: dihydrogen peroxide; sodium hydroxide / ethanol; water / 20 °C / Cooling with ice

3: copper(II) sulfate; sodium L-ascorbate; tris[(1-benzyl-1H-1,2,3-triazol-4yl)methyl]amine / water; dimethyl sulfoxide / 20 °C

With dihydrogen peroxide; copper(II) sulfate; sodium L-ascorbate; sodium hydroxide; tris[(1-benzyl-1H-1,2,3-triazol-4yl)methyl]amine; In ethanol; water; dimethyl sulfoxide; 1: Claisen-Schmidt condensation / 2: Algar-Flynn-Olyamada (AFO) reaction;
DOI:10.1016/j.bmcl.2011.03.040