2-amino-5-(1-methylethyl)-4-[3-(methyloxy)phenyl]-3-thiophenecarbonitrile

Base Information

Chemical Name:2-amino-5-(1-methylethyl)-4-[3-(methyloxy)phenyl]-3-thiophenecarbonitrile
CAS No.:1312594-22-1
Molecular Formula:C₁₅H₁₆N₂OS
Molecular Weight:272.371
Hs Code.:

Synonyms:2-amino-5-(1-methylethyl)-4-[3-(methyloxy)phenyl]-3-thiophenecarbonitrile

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Chemical Property of 2-amino-5-(1-methylethyl)-4-[3-(methyloxy)phenyl]-3-thiophenecarbonitrile

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Technology Process of 2-amino-5-(1-methylethyl)-4-[3-(methyloxy)phenyl]-3-thiophenecarbonitrile

There total 4 articles about 2-amino-5-(1-methylethyl)-4-[3-(methyloxy)phenyl]-3-thiophenecarbonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1312594-21-0
{3-methyl-1-[3-(methyloxy)phenyl]butylidene}propanedinitrile

: 1312594-22-1
2-amino-5-(1-methylethyl)-4-[3-(methyloxy)phenyl]-3-thiophenecarbonitrile

Guidance literature:: With water; sodium hydrogencarbonate; sulfur; In tetrahydrofuran; at 35 - 60 ℃;

Reference yield:

: 591-31-1
3-methoxy-benzaldehyde

: 1312594-22-1
2-amino-5-(1-methylethyl)-4-[3-(methyloxy)phenyl]-3-thiophenecarbonitrile

Guidance literature:: Multi-step reaction with 4 steps

1.1: diethyl ether / 0.17 h / 0 °C

2.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 1 h / -78 °C

2.2: 1 h / -78 °C

3.1: 1,1,1,3,3,3-hexamethyl-disilazane; acetic acid / 7 h / 70 °C

4.1: sulfur; sodium hydrogencarbonate; water / tetrahydrofuran / 35 - 60 °C

With oxalyl dichloride; water; sodium hydrogencarbonate; sulfur; acetic acid; dimethyl sulfoxide; 1,1,1,3,3,3-hexamethyl-disilazane; In tetrahydrofuran; diethyl ether; dichloromethane;

Reference yield:

: 1183770-52-6
3-methyl-1-[3-(methyloxy)phenyl]-1-butanone

: 1312594-22-1
2-amino-5-(1-methylethyl)-4-[3-(methyloxy)phenyl]-3-thiophenecarbonitrile

Guidance literature:: Multi-step reaction with 2 steps

1: 1,1,1,3,3,3-hexamethyl-disilazane; acetic acid / 7 h / 70 °C

2: sulfur; sodium hydrogencarbonate; water / tetrahydrofuran / 35 - 60 °C

With water; sodium hydrogencarbonate; sulfur; acetic acid; 1,1,1,3,3,3-hexamethyl-disilazane; In tetrahydrofuran;