3-methyl-1-[3-(methyloxy)phenyl]-1-butanone

Base Information

Chemical Name:3-methyl-1-[3-(methyloxy)phenyl]-1-butanone
CAS No.:1183770-52-6
Molecular Formula:C₁₂H₁₆O₂
Molecular Weight:192.258
Hs Code.:

Synonyms:3-methyl-1-[3-(methyloxy)phenyl]-1-butanone

Suppliers and Price of 3-methyl-1-[3-(methyloxy)phenyl]-1-butanone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Rieke Metals
1-(3-Methoxy-phenyl)-3-methyl-butan-1-one
5g
$ 927.00

Rieke Metals
1-(3-Methoxy-phenyl)-3-methyl-butan-1-one
1g
$ 527.00

Crysdot
1-(3-Methoxyphenyl)-3-methylbutan-1-one 97%
5g
$ 1215.00

Crysdot
1-(3-Methoxyphenyl)-3-methylbutan-1-one 97%
1g
$ 452.00

Total 2 raw suppliers

Chemical Property of 3-methyl-1-[3-(methyloxy)phenyl]-1-butanone

Chemical Property:

Purity/Quality:

98% ^*data from raw suppliers

1-(3-Methoxy-phenyl)-3-methyl-butan-1-one ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 3-methyl-1-[3-(methyloxy)phenyl]-1-butanone

There total 3 articles about 3-methyl-1-[3-(methyloxy)phenyl]-1-butanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 2398-37-0
3-methoxyphenyl bromide

: 147356-77-2
N-methoxy-N,3-dimethylbutanamide

: 1183770-52-6
3-methyl-1-[3-(methyloxy)phenyl]-1-butanone

Guidance literature:: 3-methoxyphenyl bromide; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.75h; Inert atmosphere;

N-methoxy-N,3-dimethylbutanamide; In tetrahydrofuran; hexane; at -78 ℃; Inert atmosphere;
DOI:10.1021/ol301332f

Reference yield: 42.0%

: 78682-47-0
1-(3-methoxyphenyl)-3-methylbutan-1-ol

: 1183770-52-6
3-methyl-1-[3-(methyloxy)phenyl]-1-butanone

Guidance literature:: With manganese(IV) oxide; In dichloromethane;

Reference yield:

: 591-31-1
3-methoxy-benzaldehyde

: 1183770-52-6
3-methyl-1-[3-(methyloxy)phenyl]-1-butanone

Guidance literature:: Multi-step reaction with 2 steps

1.1: diethyl ether / 0.17 h / 0 °C

2.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 1 h / -78 °C

2.2: 1 h / -78 °C

With oxalyl dichloride; dimethyl sulfoxide; In diethyl ether; dichloromethane;