bis(triethylphosphine)-3,3-dimethylplatinacyclobutane

Base Information

• Chemical Name: bis(triethylphosphine)-3,3-dimethylplatinacyclobutane
• CAS No.: 70620-74-5
• Molecular Formula: C₁₇H₄₀P₂Pt
• Molecular Weight: 501.532

Synonyms:bis(triethylphosphine)-3,3-dimethylplatinacyclobutane

Chemical Property of bis(triethylphosphine)-3,3-dimethylplatinacyclobutane

Chemical Property:

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Technology Process of bis(triethylphosphine)-3,3-dimethylplatinacyclobutane

There total 1 articles about bis(triethylphosphine)-3,3-dimethylplatinacyclobutane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

cis-{Pt(PEt3)2(neopentyl)2} + triethylphosphine (554-70-1) → tris(triethylphosphine)platinum(0) (39045-37-9) + 2,2,5,5-tetramethylhexane (1071-81-4) + bis(triethylphosphine)-3,3-dimethylplatinacyclobutane (70620-74-5) + 2,2-dimethylpropane (463-82-1)

Guidance literature:

In cyclohexane; (N2 or Ar); a mixture of Pt-complex and P(C2H5)3 in cyclohexane heated at 157°C for 1.6-2.25 h; cooled to -196°C; warmed to 25°C; evapd.; dissolved in acetonitrile; separated; evapd.; dissolved in ether; methanol added; cooled to -78°C; concentrated; pptd.; recrystd. from methanol/ether; elem. anal.;

DOI:10.1021/ja00542a009

upstream raw materials:

triethylphosphine

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