Technology Process of 1,3-Bis(trimethylgermyl)-2lambda~4~-diazathia-1,2-diene
There total 1 articles about 1,3-Bis(trimethylgermyl)-2lambda~4~-diazathia-1,2-diene which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
triethylamine;
In
tetrachloromethane;
under N2, N3S3Cl3 in to 50°C warmed CCl4 was added dropwise to Ge-compd. and triethylamine in CCl4 at room temp. with stirring, stirred for 20 h; filtrated, concd. (vacuum, 20 mbar), distd. (0.17 mbar): first Ge(CH3)3Cl then (CH3)3GeNSNGe(CH3)3; elem. anal.;