(1R,2S,5R)-2-isopropyl-5-methylcyclohexyl 7-(2-amino-1H-imidazol-4-yl)heptylcarbamate

Base Information

Chemical Name:(1R,2S,5R)-2-isopropyl-5-methylcyclohexyl 7-(2-amino-1H-imidazol-4-yl)heptylcarbamate
CAS No.:1279724-31-0
Molecular Formula:C₂₁H₃₈N₄O₂
Molecular Weight:378.558
Hs Code.:

Synonyms:(1R,2S,5R)-2-isopropyl-5-methylcyclohexyl 7-(2-amino-1H-imidazol-4-yl)heptylcarbamate

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Chemical Property of (1R,2S,5R)-2-isopropyl-5-methylcyclohexyl 7-(2-amino-1H-imidazol-4-yl)heptylcarbamate

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Technology Process of (1R,2S,5R)-2-isopropyl-5-methylcyclohexyl 7-(2-amino-1H-imidazol-4-yl)heptylcarbamate

There total 6 articles about (1R,2S,5R)-2-isopropyl-5-methylcyclohexyl 7-(2-amino-1H-imidazol-4-yl)heptylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1279724-30-9
tert-butyl 2-amino-4-(7-(((1R,2S,5R)-2-isopropyl-5-methylcyclohexyloxy)carbonylamino)heptyl)-1H-imidazole-1-carboxylate

: 1279724-31-0
(1R,2S,5R)-2-isopropyl-5-methylcyclohexyl 7-(2-amino-1H-imidazol-4-yl)heptylcarbamate

Guidance literature:: With trifluoroacetic acid; In dichloromethane; for 16h;
DOI:10.1016/j.bmcl.2010.12.057

Reference yield:

: 217180-77-3
8-azidooctanoyl chloride

: 1279724-31-0
(1R,2S,5R)-2-isopropyl-5-methylcyclohexyl 7-(2-amino-1H-imidazol-4-yl)heptylcarbamate

Guidance literature:: Multi-step reaction with 5 steps

1: dichloromethane / 1 h / 0 °C

2: N,N-dimethyl-formamide / 48 h

3: palladium 10% on activated carbon; hydrogen / methanol

4: triethylamine / dichloromethane / 0 - 20 °C

5: trifluoroacetic acid / dichloromethane / 16 h

With palladium 10% on activated carbon; hydrogen; triethylamine; trifluoroacetic acid; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2010.12.057

Reference yield:

: 1279724-16-1
9-azido-1-bromononan-2-one

: 1279724-31-0
(1R,2S,5R)-2-isopropyl-5-methylcyclohexyl 7-(2-amino-1H-imidazol-4-yl)heptylcarbamate

Guidance literature:: Multi-step reaction with 4 steps

1: N,N-dimethyl-formamide / 48 h

2: palladium 10% on activated carbon; hydrogen / methanol

3: triethylamine / dichloromethane / 0 - 20 °C

4: trifluoroacetic acid / dichloromethane / 16 h

With palladium 10% on activated carbon; hydrogen; triethylamine; trifluoroacetic acid; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2010.12.057