(1S,2S,4S,5S)-4-Acetoxy-5-phenylselanyl-cyclohexane-1,2-dicarboxylic acid diethyl ester

Base Information

Chemical Name:(1S,2S,4S,5S)-4-Acetoxy-5-phenylselanyl-cyclohexane-1,2-dicarboxylic acid diethyl ester
CAS No.:118374-48-4
Molecular Formula:C₂₀H₂₆O₆Se
Molecular Weight:441.383
Hs Code.:

Synonyms:(1S,2S,4S,5S)-4-Acetoxy-5-phenylselanyl-cyclohexane-1,2-dicarboxylic acid diethyl ester

Suppliers and Price of (1S,2S,4S,5S)-4-Acetoxy-5-phenylselanyl-cyclohexane-1,2-dicarboxylic acid diethyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1S,2S,4S,5S)-4-Acetoxy-5-phenylselanyl-cyclohexane-1,2-dicarboxylic acid diethyl ester

Chemical Property:

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Technology Process of (1S,2S,4S,5S)-4-Acetoxy-5-phenylselanyl-cyclohexane-1,2-dicarboxylic acid diethyl ester

There total 1 articles about (1S,2S,4S,5S)-4-Acetoxy-5-phenylselanyl-cyclohexane-1,2-dicarboxylic acid diethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 34837-55-3
Phenylselenyl bromide

: 4841-85-4,5048-50-0,13043-60-2,56000-17-0
trans-1,2-bis(ethoxycarbonyl)-4-cyclohexene

: 64-19-7,77671-22-8
acetic acid

: 118374-48-4
(1S,2S,4S,5S)-4-Acetoxy-5-phenylselanyl-cyclohexane-1,2-dicarboxylic acid diethyl ester

Guidance literature:: With potassium acetate; acetic anhydride; for 15.5h; Ambient temperature;
DOI:10.1021/jo00265a031

Reference yield: 91.0%

: 118374-48-4
(1S,2S,4S,5S)-4-Acetoxy-5-phenylselanyl-cyclohexane-1,2-dicarboxylic acid diethyl ester

: 118374-49-5
C₂₀H₂₆Cl₂O₆Se

Guidance literature:: With sulfuryl dichloride; In chloroform; for 0.25h; Ambient temperature;
DOI:10.1021/jo00265a031

Reference yield:

: 118374-48-4
(1S,2S,4S,5S)-4-Acetoxy-5-phenylselanyl-cyclohexane-1,2-dicarboxylic acid diethyl ester

: 118270-85-2
(1S,2S,5S)-5-Acetoxy-cyclohex-3-ene-1,2-dicarboxylic acid diethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 91 percent / SO₂Cl₂ / CHCl₃ / 0.25 h / Ambient temperature

2: NaHCO₃, water / CH₂Cl₂

3: NaHCO₃, water / CH₂Cl₂ / 120 h / Ambient temperature

With sulfuryl dichloride; water; sodium hydrogencarbonate; In dichloromethane; chloroform;
DOI:10.1021/jo00265a031