[(2,6-iPr₂C₆H₃NC(Me)C(Me)NC-2,6-iPr₂C₆H₃)Pd(CH₂)3C(O)OMe](B(3,5-C₆H₃(CF₃)2)4)

Base Information

Chemical Name:[(2,6-iPr₂C₆H₃NC(Me)C(Me)NC-2,6-iPr₂C₆H₃)Pd(CH₂)3C(O)OMe](B(3,5-C₆H₃(CF₃)2)4)
CAS No.:171901-49-8
Molecular Formula:C₃₂H₁₂BF₂₄*C₃₃H₄₉N₂O₂Pd
Molecular Weight:1475.4
Hs Code.:

[(2,6-iPr<sub>2</sub>C<sub>6</sub>H<sub>3</sub>NC(Me)C(Me)NC-2,6-iPr<sub>2</sub>C<sub>6</sub>H<sub>3</sub>)Pd(CH<sub>2</sub>)3C(O)OMe](B(3,5-C<sub>6</sub>H<sub>3</sub>(CF<sub>3</sub>)2)4)

Synonyms:[(2,6-iPr₂C₆H₃NC(Me)C(Me)NC-2,6-iPr₂C₆H₃)Pd(CH₂)3C(O)OMe](B(3,5-C₆H₃(CF₃)2)4)

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Chemical Property of [(2,6-iPr₂C₆H₃NC(Me)C(Me)NC-2,6-iPr₂C₆H₃)Pd(CH₂)3C(O)OMe](B(3,5-C₆H₃(CF₃)2)4)

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Technology Process of [(2,6-iPr₂C₆H₃NC(Me)C(Me)NC-2,6-iPr₂C₆H₃)Pd(CH₂)3C(O)OMe](B(3,5-C₆H₃(CF₃)2)4)

There total 1 articles about [(2,6-iPr₂C₆H₃NC(Me)C(Me)NC-2,6-iPr₂C₆H₃)Pd(CH₂)3C(O)OMe](B(3,5-C₆H₃(CF₃)2)4) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: [(2,6-iPrC₆H₃NC(Me)C(Me)N-2,6-iPrC₆H₃)Pd(CH₃)(Cl)]

: 79060-88-1
sodium tetrakis[(3,5-di-trifluoromethyl)phenyl]borate

: 292638-85-8,9003-21-8,96-33-3
acrylic acid methyl ester

: 181709-52-4
((((CH₃)2CH)2C₆H₃NCCH₃)2PdCHCH₂CH₃C(O)OCH₃)⁽¹⁺⁾*B(C₆H₃(CF₃)2)4^(1-) = [(C₂₈H₄₀N₂)Pd(C₅H₉O₂)][B(C₈H₃F₆)4]

: 201007-41-2
((((CH₃)2CH)2C₆H₃NCCH₃)2PdCHCH₂CH₃C(O)OCH₃)⁽¹⁺⁾*B(C₆H₃(CF₃)2)4^(1-)=[(C₂₈H₄₀N₂)PdCHCH₂CH₃C(O)OCH₃][B(C₆H₃(CF₃)2)4]

: 171901-49-8
[(2,6-iPr₂C₆H₃NC(Me)C(Me)NC-2,6-iPr₂C₆H₃)Pd(CH₂)3C(O)OMe](B(3,5-C₆H₃(CF₃)2)4)

Guidance literature:: In diethyl ether; byproducts: NaCl; inert atm.; stirring (2 days), room temp.; recrystn. (CH2Cl2, -30°C), filtn (NaCl removal); products not sepd. ; elem. anal.;
DOI:10.1021/ja964144i

Reference yield:

: 2564-83-2,45842-10-2,126517-51-9,25657-03-8,26933-82-4,54637-06-8,64104-42-3
2,2,6,6-Tetramethyl-1-piperidinyloxy free radical

: 171901-49-8
[(2,6-iPr₂C₆H₃NC(Me)C(Me)NC-2,6-iPr₂C₆H₃)Pd(CH₂)3C(O)OMe](B(3,5-C₆H₃(CF₃)2)4)

: C₃₇H₅₈N₃OPd⁽¹⁺⁾*C₃₂H₁₂BF₂₄^(1-)

Guidance literature:: With acrylic acid methyl ester; In dichloromethane; at 25 - 27 ℃; for 18h; Solvent; Inert atmosphere; Irradiation; Glovebox;
DOI:10.1021/jacs.0c10588