N-[4-(carboxy)benzylidene]-N-[1,1-dimethyl-2-(N-octanoyl)amido]ethylamine N-oxide

Base Information

Chemical Name:N-[4-(carboxy)benzylidene]-N-[1,1-dimethyl-2-(N-octanoyl)amido]ethylamine N-oxide
CAS No.:946148-83-0
Molecular Formula:C₂₀H₃₀N₂O₄
Molecular Weight:362.469
Hs Code.:

Synonyms:N-[4-(carboxy)benzylidene]-N-[1,1-dimethyl-2-(N-octanoyl)amido]ethylamine N-oxide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-[4-(carboxy)benzylidene]-N-[1,1-dimethyl-2-(N-octanoyl)amido]ethylamine N-oxide

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Technology Process of N-[4-(carboxy)benzylidene]-N-[1,1-dimethyl-2-(N-octanoyl)amido]ethylamine N-oxide

There total 1 articles about N-[4-(carboxy)benzylidene]-N-[1,1-dimethyl-2-(N-octanoyl)amido]ethylamine N-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 619-66-9
4-Carboxybenzaldehyde

: 549505-85-3
octanoic acid (2-hydroxyamino-2-methyl-propyl)-amide

: 946148-83-0
N-[4-(carboxy)benzylidene]-N-[1,1-dimethyl-2-(N-octanoyl)amido]ethylamine N-oxide

Guidance literature:: In pyridine; ethanol; at 65 ℃; for 48h;
DOI:10.1021/jm0706968

Reference yield: 42.0%

: 946148-83-0
N-[4-(carboxy)benzylidene]-N-[1,1-dimethyl-2-(N-octanoyl)amido]ethylamine N-oxide

: 6066-82-6
1-hydroxy-pyrrolidine-2,5-dione

: 946148-80-7
N-[4-(succinimidocarboxy)benzylidene]-N-[1,1-dimethyl-2-(N-octanoyl)amido]ethylamine N-oxide

Guidance literature:: With dicyclohexyl-carbodiimide; In dichloromethane; for 24h;
DOI:10.1021/jm0706968

Reference yield:

: 946148-83-0
N-[4-(carboxy)benzylidene]-N-[1,1-dimethyl-2-(N-octanoyl)amido]ethylamine N-oxide

: C₂₆H₄₂N₄O₇

Guidance literature:: Multi-step reaction with 3 steps

1: 42 percent / dicyclohexylcarbodiimide / CH₂Cl₂ / 24 h

2: 79 percent / diisopropylethylamine / CH₂Cl₂ / 48 h / 20 °C / pH 8 - 9

3: 56 percent / methanol / sodium methoxide / 8 h

With methanol; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide; sodium methylate; In dichloromethane;
DOI:10.1021/jm0706968