5-O-tert-butyldimethylsilyl-1-deoxy-3,4-O-isopropylidene-1-phenylthio-D-erythro-pentulose

Base Information

Chemical Name:5-O-tert-butyldimethylsilyl-1-deoxy-3,4-O-isopropylidene-1-phenylthio-D-erythro-pentulose
CAS No.:129034-03-3
Molecular Formula:C₂₀H₃₂O₄SSi
Molecular Weight:396.623
Hs Code.:

Synonyms:5-O-tert-butyldimethylsilyl-1-deoxy-3,4-O-isopropylidene-1-phenylthio-D-erythro-pentulose

Suppliers and Price of 5-O-tert-butyldimethylsilyl-1-deoxy-3,4-O-isopropylidene-1-phenylthio-D-erythro-pentulose

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 5-O-tert-butyldimethylsilyl-1-deoxy-3,4-O-isopropylidene-1-phenylthio-D-erythro-pentulose

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 5-O-tert-butyldimethylsilyl-1-deoxy-3,4-O-isopropylidene-1-phenylthio-D-erythro-pentulose

There total 7 articles about 5-O-tert-butyldimethylsilyl-1-deoxy-3,4-O-isopropylidene-1-phenylthio-D-erythro-pentulose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 129034-02-2
1-O-tert-butyldimethylsilyl-5-deoxy-2,3-O-isopropylidene-5-phenylthio-D-lyxitol

: 129034-03-3
5-O-tert-butyldimethylsilyl-1-deoxy-3,4-O-isopropylidene-1-phenylthio-D-erythro-pentulose

Guidance literature:: With pyridine; dimethyl sulfoxide; dicyclohexyl-carbodiimide; trifluoroacetic acid; In diethyl ether; 0 deg C then RT, 3 h;

Reference yield:

: 129034-01-1
5-deoxy-2,3-O-isopropylidene-5-phenylthio-D-lyxitol

: 129034-03-3
5-O-tert-butyldimethylsilyl-1-deoxy-3,4-O-isopropylidene-1-phenylthio-D-erythro-pentulose

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / imidazole / dimethylformamide / 0.75 h / Ambient temperature

2: 98 percent / DMSO, dicyclohexyl carbodiimide, pyridine, trifluoroacetic acid / diethyl ether / 0 deg C then RT, 3 h

With pyridine; 1H-imidazole; dimethyl sulfoxide; dicyclohexyl-carbodiimide; trifluoroacetic acid; In diethyl ether; N,N-dimethyl-formamide;

Reference yield:

: 129034-00-0
5-deoxy-2,3-O-isopropylidene-5-phenylthio-α-D-lyxofuranose

: 129034-03-3
5-O-tert-butyldimethylsilyl-1-deoxy-3,4-O-isopropylidene-1-phenylthio-D-erythro-pentulose

Guidance literature:: Multi-step reaction with 3 steps

1: 83 percent / NaBH₄ / methanol / 3 h

2: 92 percent / imidazole / dimethylformamide / 0.75 h / Ambient temperature

3: 98 percent / DMSO, dicyclohexyl carbodiimide, pyridine, trifluoroacetic acid / diethyl ether / 0 deg C then RT, 3 h

With pyridine; 1H-imidazole; sodium tetrahydroborate; dimethyl sulfoxide; dicyclohexyl-carbodiimide; trifluoroacetic acid; In methanol; diethyl ether; N,N-dimethyl-formamide;