C₁₄H₁₈ClN₃O₂

Base Information

Chemical Name:C₁₄H₁₈ClN₃O₂
CAS No.:1404376-40-4
Molecular Formula:C₁₄H₁₈ClN₃O₂
Molecular Weight:295.769
Hs Code.:

C<sub>14</sub>H<sub>18</sub>ClN<sub>3</sub>O<sub>2</sub>

Synonyms:C₁₄H₁₈ClN₃O₂

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Chemical Property of C₁₄H₁₈ClN₃O₂

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Technology Process of C₁₄H₁₈ClN₃O₂

There total 1 articles about C₁₄H₁₈ClN₃O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 89896-39-9
ethyl 5-azidovalerate

: 622-95-7
4-chlorobenzyl bromide

: 1404376-40-4
C₁₄H₁₈ClN₃O₂

Guidance literature:: ethyl 5-azidovalerate; With n-butyllithium; diisopropylamine; In tetrahydrofuran; hexane; at -78 ℃; for 0.5h; Inert atmosphere;

4-chlorobenzyl bromide; With N,N,N,N,N,N-hexamethylphosphoric triamide; In tetrahydrofuran; hexane; at -78 - 20 ℃; for 15h; Inert atmosphere;
DOI:10.1021/ol302890a

Reference yield: 69.0%

: 1404376-40-4
C₁₄H₁₈ClN₃O₂

: 1404376-13-1
C₁₂H₁₄ClN₃O₂

Guidance literature:: C₁₄H₁₈ClN₃O₂; With lithium hydroxide; In tetrahydrofuran; water; at 20 - 66 ℃; for 24h; Inert atmosphere;

With sulfuric acid; at 20 ℃; pH=3 - 4; Inert atmosphere;
DOI:10.1021/ol302890a

Reference yield:

: 1404376-40-4
C₁₄H₁₈ClN₃O₂

: C₁₂H₁₃Cl₂N₃O

Guidance literature:: Multi-step reaction with 2 steps

1.1: lithium hydroxide / tetrahydrofuran; water / 24 h / 20 - 66 °C / Inert atmosphere

1.2: 20 °C / pH 3 - 4 / Inert atmosphere

2.1: oxalyl dichloride / dichloromethane / 1 h / 20 °C / Inert atmosphere

With oxalyl dichloride; lithium hydroxide; In tetrahydrofuran; dichloromethane; water;
DOI:10.1021/ol302890a