C₉H₈ClF₃O₃S

Base Information

Chemical Name:C₉H₈ClF₃O₃S
CAS No.:1320208-50-1
Molecular Formula:C₉H₈ClF₃O₃S
Molecular Weight:288.675
Hs Code.:

C<sub>9</sub>H<sub>8</sub>ClF<sub>3</sub>O<sub>3</sub>S

Synonyms:C₉H₈ClF₃O₃S

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₉H₈ClF₃O₃S

Chemical Property:

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Technology Process of C₉H₈ClF₃O₃S

There total 3 articles about C₉H₈ClF₃O₃S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 1320208-49-8
C₉H₉F₃OS

: 1320208-50-1
C₉H₈ClF₃O₃S

Guidance literature:: With sulfuryl dichloride; potassium nitrate; In acetonitrile; at 0 ℃;
DOI:10.1021/jo200958a

Reference yield:

: 122243-30-5
2-(3-bromophenyl)-1,1,1-trifluoropropan-2-ol

: 1320208-50-1
C₉H₈ClF₃O₃S

Guidance literature:: Multi-step reaction with 2 steps

1: palladium diacetate; caesium carbonate; triphenylphosphine; triisopropylsilanethiol / toluene / 100 °C

2: sulfuryl dichloride; potassium nitrate / acetonitrile / 0 °C

With sulfuryl dichloride; palladium diacetate; caesium carbonate; potassium nitrate; triphenylphosphine; triisopropylsilanethiol; In toluene; acetonitrile;
DOI:10.1021/jo200958a

Reference yield:

: 2142-63-4
1-(3-Bromophenyl)ethanone

: 1320208-50-1
C₉H₈ClF₃O₃S

Guidance literature:: Multi-step reaction with 3 steps

1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0 - 20 °C

2: palladium diacetate; caesium carbonate; triphenylphosphine; triisopropylsilanethiol / toluene / 100 °C

3: sulfuryl dichloride; potassium nitrate / acetonitrile / 0 °C

With sulfuryl dichloride; tetrabutyl ammonium fluoride; palladium diacetate; caesium carbonate; potassium nitrate; triphenylphosphine; triisopropylsilanethiol; In tetrahydrofuran; toluene; acetonitrile;
DOI:10.1021/jo200958a