ζ,ζ-diphenyl-ζ-(1-tricyclo[3.3.1.1.(3,7)]decane)hexanol

Base Information

Chemical Name:ζ,ζ-diphenyl-ζ-(1-tricyclo[3.3.1.1.(3,7)]decane)hexanol
CAS No.:1427162-86-4
Molecular Formula:C₂₈H₃₆O
Molecular Weight:388.593
Hs Code.:

Synonyms:ζ,ζ-diphenyl-ζ-(1-tricyclo[3.3.1.1.(3,7)]decane)hexanol

Suppliers and Price of ζ,ζ-diphenyl-ζ-(1-tricyclo[3.3.1.1.(3,7)]decane)hexanol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of ζ,ζ-diphenyl-ζ-(1-tricyclo[3.3.1.1.(3,7)]decane)hexanol

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of ζ,ζ-diphenyl-ζ-(1-tricyclo[3.3.1.1.(3,7)]decane)hexanol

There total 3 articles about ζ,ζ-diphenyl-ζ-(1-tricyclo[3.3.1.1.(3,7)]decane)hexanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 1427162-91-1
ethyl ε,ε-diphenyl-ε-(1-tricyclo[3.3.1.1.(3,7)]decane)hexanoate

: 1427162-86-4
ζ,ζ-diphenyl-ζ-(1-tricyclo[3.3.1.1.(3,7)]decane)hexanol

Guidance literature:: ethyl ε,ε-diphenyl-ε-(1-tricyclo[3.3.1.1.(3,7)]decane)hexanoate; With lithium aluminium tetrahydride; In tetrahydrofuran; at 20 ℃; for 1h;

With water; sodium hydroxide; In ethanol; water; at 0 ℃;
DOI:10.2174/157340612801216201

Reference yield:

: 66951-99-3
α,α-diphenyl-1-tricyclo[3.3.1.1.(3,7)]decanemethanol

: 1427162-86-4
ζ,ζ-diphenyl-ζ-(1-tricyclo[3.3.1.1.(3,7)]decane)hexanol

Guidance literature:: Multi-step reaction with 6 steps

1.1: thionyl chloride; acetyl chloride / 0.5 h / Reflux

2.1: copper(l) iodide / tetrahydrofuran / 4 h / Inert atmosphere; Reflux

2.2: 0 °C / Inert atmosphere

3.1: pyridinium chlorochromate / dichloromethane / 2 h / 20 °C

4.1: sodium hydride / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

4.2: 0.5 h / 0 °C / Inert atmosphere

5.1: palladium 10% on activated carbon; hydrogen / ethanol / 16 h / 20 °C

6.1: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / 20 °C

6.2: 0 °C

With copper(l) iodide; lithium aluminium tetrahydride; thionyl chloride; palladium 10% on activated carbon; hydrogen; sodium hydride; acetyl chloride; pyridinium chlorochromate; In tetrahydrofuran; ethanol; dichloromethane;
DOI:10.2174/157340612801216201

Reference yield:

: 51046-41-4
α,α-diphenyl-1-tricyclo[3.3.1.1.(3,7)]decylmethyl chloride

: 1427162-86-4
ζ,ζ-diphenyl-ζ-(1-tricyclo[3.3.1.1.(3,7)]decane)hexanol

Guidance literature:: Multi-step reaction with 5 steps

1.1: copper(l) iodide / tetrahydrofuran / 4 h / Inert atmosphere; Reflux

1.2: 0 °C / Inert atmosphere

2.1: pyridinium chlorochromate / dichloromethane / 2 h / 20 °C

3.1: sodium hydride / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

3.2: 0.5 h / 0 °C / Inert atmosphere

4.1: palladium 10% on activated carbon; hydrogen / ethanol / 16 h / 20 °C

5.1: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / 20 °C

5.2: 0 °C

With copper(l) iodide; lithium aluminium tetrahydride; palladium 10% on activated carbon; hydrogen; sodium hydride; pyridinium chlorochromate; In tetrahydrofuran; ethanol; dichloromethane;
DOI:10.2174/157340612801216201