N-(4'-Iodobiphenyl-4-yl)-N-(m-tolyl)aniline

Base Information

Chemical Name:N-(4'-Iodobiphenyl-4-yl)-N-(m-tolyl)aniline
CAS No.:195443-34-6
Molecular Formula:C25H20IN
Molecular Weight:461.345
Hs Code.:2921499090
European Community (EC) Number:678-558-5
DSSTox Substance ID:DTXSID50443908
Wikidata:Q72483473
Mol file:195443-34-6.mol

Synonyms:195443-34-6;N-(4'-Iodobiphenyl-4-yl)-N-(m-tolyl)aniline;4'-Iodo-N-phenyl-N-(m-tolyl)-[1,1'-biphenyl]-4-amine;N-(4'-IODOBIPHENYL-4-YL)-N-(3-METHYLPHENYL)ANILINE;N-[4-(4-iodophenyl)phenyl]-3-methyl-N-phenylaniline;N-(4/'-Iodobiphenyl-4-yl)-N-(3-methylphenyl)aniline;SCHEMBL5357367;DTXSID50443908;AKQZSFMSAULQQN-UHFFFAOYSA-N;MFCD00671551;AS-69059;4'-iodo-N-phenyl-N-m-tolyl-4-aminobiphenyl;I0490;N-(4-Iodobiphenyl-4-yl)-N-(m-tolyl)aniline;T72015;4'-Iodo-4-[N-phenyl-N-(m-tolyl)amino]biphenyl;N-(4/'-Iodobiphenyl-4-yl)-N-(m-tolyl)aniline;A813807;N-(4'-Iodobiphenyl-4-yl)-N-phenyl-N-(m-tolyl)amine;4'-Iodo-N-(3-methylphenyl)-N-phenyl[1,1'-biphenyl]-4-amine;4'-IODO-N-(3-METHYLPHENYL)-N-PHENYL-[1,1'-BIPHENYL]-4-AMINE

Suppliers and Price of N-(4'-Iodobiphenyl-4-yl)-N-(m-tolyl)aniline

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TCI Chemical
N-(4'-Iodobiphenyl-4-yl)-N-(m-tolyl)aniline >98.0%(HPLC)
1g
$ 709.00

Crysdot
4'-Iodo-N-phenyl-N-(m-tolyl)-[1,1'-biphenyl]-4-amine 95+%
1g
$ 459.00

American Custom Chemicals Corporation
N-(4'-IODOBIPHENYL-4-YL)-N-(3-METHYLPHENYL)ANILINE 95.00%
1G
$ 617.40

Alichem
4'-Iodo-N-phenyl-N-(m-tolyl)-[1,1'-biphenyl]-4-amine
1g
$ 487.20

AK Scientific
N-(4'-Iodobiphenyl-4-yl)-N-(3-methylphenyl)aniline
1g
$ 1001.00

Total 13 raw suppliers

Chemical Property of N-(4'-Iodobiphenyl-4-yl)-N-(m-tolyl)aniline

Chemical Property:

Appearance/Colour:White to light yellow crystalline powder
Vapor Pressure:0mmHg at 25°C
Melting Point:160 °C
Refractive Index:1.679
Boiling Point:550.588 °C at 760 mmHg
Flash Point:286.786 °C
PSA：3.24000
Density:1.423 g/cm³
LogP:7.73640
XLogP3:7.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:4
Exact Mass:461.06405
Heavy Atom Count:27
Complexity:430

Purity/Quality:

97% ^*data from raw suppliers

N-(4'-Iodobiphenyl-4-yl)-N-(m-tolyl)aniline >98.0%(HPLC) ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC(=CC=C1)N(C2=CC=CC=C2)C3=CC=C(C=C3)C4=CC=C(C=C4)I

Technology Process of N-(4'-Iodobiphenyl-4-yl)-N-(m-tolyl)aniline

There total 3 articles about N-(4'-Iodobiphenyl-4-yl)-N-(m-tolyl)aniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 204327-05-9
N-(3-methylphenyl)-N-phenyl-4-bromo-1,1'-biphenyl-4'-amine

: 195443-34-6
N-(3-methylphenyl)-N-phenyl-4-iodo-1,1'-biphenyl-4'-amine

Guidance literature:: N-(3-methylphenyl)-N-phenyl-4-bromo-1,1'-biphenyl-4'-amine; With n-butyllithium; In diethyl ether; cyclohexane; at 20 ℃; for 1h;

With iodine; In diethyl ether; cyclohexane; at 0 ℃;
DOI:10.1021/jo981804o

Reference yield:

: 1205-64-7
3-Methyldiphenylamine

: 195443-34-6
N-(3-methylphenyl)-N-phenyl-4-iodo-1,1'-biphenyl-4'-amine

Guidance literature:: Multi-step reaction with 2 steps

1.1: 80 percent / 1,10-phenanthroline; cuprous chloride; potassium hydroxide / toluene / 5 h / 125 °C

2.1: n-butyllithium / diethyl ether; cyclohexane / 1 h / 20 °C

2.2: iodine / diethyl ether; cyclohexane / 0 °C

With potassium hydroxide; n-butyllithium; 1,10-Phenanthroline; copper(l) chloride; In diethyl ether; cyclohexane; toluene; 1.1: Ullmann condensation / 2.1: Metallation / 2.2: Iodination;
DOI:10.1021/jo981804o

Reference yield:

: 105946-82-5
4-bromo-4'-iodobiphenyl

: 195443-34-6
N-(3-methylphenyl)-N-phenyl-4-iodo-1,1'-biphenyl-4'-amine

Guidance literature:: Multi-step reaction with 2 steps

1.1: 80 percent / 1,10-phenanthroline; cuprous chloride; potassium hydroxide / toluene / 5 h / 125 °C

2.1: n-butyllithium / diethyl ether; cyclohexane / 1 h / 20 °C

2.2: iodine / diethyl ether; cyclohexane / 0 °C

With potassium hydroxide; n-butyllithium; 1,10-Phenanthroline; copper(l) chloride; In diethyl ether; cyclohexane; toluene; 1.1: Ullmann condensation / 2.1: Metallation / 2.2: Iodination;
DOI:10.1021/jo981804o